meso-Tetra (N-methyl-3-pyridyl) porphine tetrachloride

Base Information

• Chemical Name: meso-Tetra (N-methyl-3-pyridyl) porphine tetrachloride
• CAS No.: 94343-62-1
• Molecular Formula: C₄₄H₃₈N₈*4Cl
• Molecular Weight: 820.651
• Mol file: 94343-62-1.mol

Synonyms:meso-Tetra (N-methyl-3-pyridyl) porphine tetrachloride

Chemical Property of meso-Tetra (N-methyl-3-pyridyl) porphine tetrachloride

Chemical Property:

• PSA: 71.82000
• LogP: -9.81980

Purity/Quality:

98% purity ^*data from raw suppliers

meso-Tetra(N-Methyl-3-pyridyl)PorphineTetrachloride ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Uses: meso-Tetra (N-methyl-3-pyridyl) porphine tetrachloride is a synthetic porphyrin.

Technology Process of meso-Tetra (N-methyl-3-pyridyl) porphine tetrachloride

There total 3 articles about meso-Tetra (N-methyl-3-pyridyl) porphine tetrachloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

5,10,15,20-tetra(3-pyridyl)porphyrin (40882-83-5) + methyl p-toluene sulfonate (80-48-8) → dihydrogen meso-tetra(N-methyl-3-pyridyl)porphyrin tetrachloride (94343-62-1)

Guidance literature:

In N,N-dimethyl-formamide; at 112 ℃;

DOI:10.1021/ic3012519

Reference yield:

5,10,15,20-tetrakis(1'-methyl-pyrid-3-yl)porphyrin tetraiodide → dihydrogen meso-tetra(N-methyl-3-pyridyl)porphyrin tetrachloride (94343-62-1)

Guidance literature:

Multi-step reaction with 2 steps

1: ammonium hexafluorophosphate / water

2: tetrabutyl-ammonium chloride / acetone

With ammonium hexafluorophosphate; tetrabutyl-ammonium chloride; In water; acetone;

DOI:10.3390/ijms21155367

Reference yield:

C44H38N8(4+)*4F6P(1-) → dihydrogen meso-tetra(N-methyl-3-pyridyl)porphyrin tetrachloride (94343-62-1)

Guidance literature:

With tetrabutyl-ammonium chloride; In acetone;

DOI:10.3390/ijms21155367

upstream raw materials:

5,10,15,20-tetra(3-pyridyl)porphyrin

methyl p-toluene sulfonate

Refernces

• 1、 Tovmasyan, Artak,Weitner, Tin,Sheng, Huaxin,Lu, Miaomiao,Rajic, Zrinka,Warner, David S.,Spasojevic, Ivan,Reboucas, Julio S.,Benov, Ludmil,Batinic-Haberle, Ines. "Differential coordination demands in Fe versus Mn water-soluble cationic metalloporphyrins translate into remarkably different aqueous redox chemistry and biology". . p. 5677 - 5691. Retrieved 2013/07/11.