Bis[tris(trimethylsilyl)silyl]zinc

Base Information

Chemical Name:Bis[tris(trimethylsilyl)silyl]zinc
CAS No.:108168-22-5
Molecular Formula:C18H54Si8Zn
Molecular Weight:560.701
Hs Code.:
Mol file:108168-22-5.mol

Synonyms:Bis[tris(trimethylsilyl)silyl]zinc

Suppliers and Price of Bis[tris(trimethylsilyl)silyl]zinc

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Total 1 raw suppliers

Chemical Property of Bis[tris(trimethylsilyl)silyl]zinc

Chemical Property:

Melting Point:194 - 195 °C
PSA：0.00000
LogP:7.45950

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of Bis[tris(trimethylsilyl)silyl]zinc

There total 4 articles about Bis[tris(trimethylsilyl)silyl]zinc which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1873-77-4
tris-(trimethylsilyl)silane

: 557-20-0
diethylzinc

: 108168-22-5
bis[tris(trimethylsilyl)silyl]zinc

Guidance literature:: With AIBN or tBu₂Hg; at 60°C for 20 min;
DOI:10.1002/anie.201200126

Reference yield: 81.0%

: tris(trimethylsilyl)silyl lithium * 3 tetrahydrofuran

: 7646-85-7,24359-56-6
zinc(II) chloride

: 108168-22-5
bis[tris(trimethylsilyl)silyl]zinc

Guidance literature:: In diethyl ether; a soln. of ZnCl2 and (THF)3LiSi(SiMe3)3 in diethyl ether was stirred at room temp. for 10 h; volatiles were removed under vac., residue was extd. into pentane, mixt. was concd. and cooled to -45°C for 12 h; elem.anal.;

Reference yield: 50.0%

: tris(trimethylsilyl)silyllithium*3(tetrahydrofuran)

: [tris(trimethylsilyl)germyl]zinc chloride mono-tetrahydrofuran solvate

: bis[tris(trimethylsilyl)germyl]zinc

: 108168-22-5
bis[tris(trimethylsilyl)silyl]zinc

: (Me₃Si)3GeZnSi(SiMe₃)3

Guidance literature:: In tetrahydrofuran; under Ar; THF soln. of SiLi deriv. and germylzinc stirred at room temp. for 2 h;
DOI:10.1016/S0022-328X(03)00148-7