Carbamic acid, 3,4-pentadienyl-, 1,1-dimethylethyl ester (9CI)

Base Information

Chemical Name:Carbamic acid, 3,4-pentadienyl-, 1,1-dimethylethyl ester (9CI)
CAS No.:363599-38-6
Molecular Formula:C₁₀H₁₇NO₂
Molecular Weight:183.25
Hs Code.:
Mol file:363599-38-6.mol

Synonyms:Carbamic acid, 3,4-pentadienyl-, 1,1-dimethylethyl ester (9CI)

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Chemical Property of Carbamic acid, 3,4-pentadienyl-, 1,1-dimethylethyl ester (9CI)

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Technology Process of Carbamic acid, 3,4-pentadienyl-, 1,1-dimethylethyl ester (9CI)

There total 3 articles about Carbamic acid, 3,4-pentadienyl-, 1,1-dimethylethyl ester (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 149990-27-2
tert-butyl but-3-yn-1-ylcarbamate

: 363599-38-6
N-(tert-Butoxycarbonyl)penta-3,4-dienylamine

Guidance literature:: With diisopropylamine; copper(I) bromide; In 1,4-dioxane; Reflux;
DOI:10.1021/ol101425y

Reference yield: 63.0%

: 122234-46-2
2-iodo-1-<(tert-butyloxycarbonyl)amino>ethane

: 624-65-7
2-propynyl chloride

: 363599-38-6
N-(tert-Butoxycarbonyl)penta-3,4-dienylamine

Guidance literature:: 2-iodo-1-<(tert-butyloxycarbonyl)amino>ethane; With chloro-trimethyl-silane; zinc; In N,N-dimethyl-formamide; at 0 ℃;

2-propynyl chloride; With copper(I) bromide dimethylsulfide complex; In N,N-dimethyl-formamide; at 20 ℃; for 14h; Further stages.;
DOI:10.1039/b102446a

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 363599-38-6
N-(tert-Butoxycarbonyl)penta-3,4-dienylamine

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydrogencarbonate / water / 0.17 h / 0 - 25 °C / Inert atmosphere

1.2: 12 h / 0 - 25 °C / Inert atmosphere

2.1: copper(I) bromide; diisopropylamine / 1,4-dioxane / 14 h / Inert atmosphere; Reflux

With sodium hydrogencarbonate; diisopropylamine; copper(I) bromide; In 1,4-dioxane; water;
DOI:10.1002/anie.202101439