Allyl dithiopropanoate

Base Information

• Chemical Name: Allyl dithiopropanoate
• CAS No.: 41830-43-7
• Molecular Formula: C₆H₁₀S₂
• Molecular Weight: 146.277
• Hs Code.: 2930909090
• Mol file: 41830-43-7.mol

Synonyms:Allyl dithiopropanoate

Chemical Property of Allyl dithiopropanoate

Chemical Property:

• Boiling Point: 96-97 °C(Press: 12 Torr)
• PSA: 57.39000
• Density: 1.032±0.06 g/cm3(Predicted)
• LogP: 2.64300

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Allyl dithiopropanoate

There total 3 articles about Allyl dithiopropanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

dithiopropionic acid (1892-30-4) + allyl alcohol (107-18-6) → dithiopropionic acid allyl ester (41830-43-7)

Guidance literature:

With di-isopropyl azodicarboxylate; triphenylphosphine; In tetrahydrofuran; at 0 ℃; for 0.5h;

DOI:10.1055/s-1989-27177

Reference yield:

carbon disulfide (75-15-0,12122-00-8) + ethylmagnesium bromide (925-90-6) + allyl bromide (106-95-6) → dithiopropionic acid allyl ester (41830-43-7)

Guidance literature:

Multistep reaction; (i) THF, (ii) /BRN= 605308/;

Reference yield:

C15H33NO6*2C2H5BrMg + allylmagnesium bromide (1730-25-2) → dithiopropionic acid allyl ester (41830-43-7)

Guidance literature:

Yield given. Multistep reaction; 1.) THF, 20 deg C; 2.) THF;

DOI:10.1016/0040-4020(89)80044-4

upstream raw materials:

carbon disulfide

ethylmagnesium bromide

allyl bromide

dithiopropionic acid

Refernces

• 1、 Kpegba, Kafui,Metzner, Patrick. "Synthesis of Dithioic Acid Esters by a Mitsunobu-Type Reaction of Alkanedithioic Acids and Alcohols". . p. 137 - 139. Retrieved 2007/10/02.