(2,3-dichlorophenoxy)acetyl chloride

Base Information

• Chemical Name: (2,3-dichlorophenoxy)acetyl chloride
• CAS No.: 85630-84-8
• Molecular Formula: C8H5Cl3O2
• Molecular Weight: 239.485
• Mol file: 85630-84-8.mol

Synonyms:(2,3-dichlorophenoxy)acetyl chloride;acetyl chloride, (2,3-dichlorophenoxy)-;2-(2,3-dichlorophenoxy)acetyl chloride;2-(2,3-dichlorophenoxy)ethanoyl chloride

Chemical Property of (2,3-dichlorophenoxy)acetyl chloride

Chemical Property:

• Melting Point: 171-173 °C
• Boiling Point: 298.8±25.0 °C(Predicted)
• Density: 1.475±0.06 g/cm3(Predicted)

Purity/Quality:

99%, ^*data from raw suppliers

(2,3-Dichlorophenoxy)acetyl chloride ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of (2,3-dichlorophenoxy)acetyl chloride

There total 2 articles about (2,3-dichlorophenoxy)acetyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2,3-dichlorophenoxyacetic acid (2976-74-1) → (2,3-dichlorophenoxy)acetyl chloride (85630-84-8)

Guidance literature:

With thionyl chloride;

DOI:10.1023/A:1012387131029

Reference yield:

2,3-dichlorophenol (576-24-9) → (2,3-dichlorophenoxy)acetyl chloride (85630-84-8)

Guidance literature:

Multi-step reaction with 2 steps

1: 77 percent / NaOH / H₂O / 3 h / 110 - 120 °C

2: SOCl₂

With sodium hydroxide; thionyl chloride; In water;

DOI:10.1023/A:1012387131029

Reference yield: 78.0%

Geraniol (106-24-1) + (2,3-dichlorophenoxy)acetyl chloride (85630-84-8) → geranyl (2,3-dichlorophenoxy)acetate

Guidance literature:

In benzene; for 0.5h;

DOI:10.1023/A:1012387131029

upstream raw materials:

2,3-dichlorophenoxyacetic acid

2,3-dichlorophenol

Downstream raw materials:

5-Chloro-4-[2-(2,3-dichloro-phenoxy)-acetylamino]-N-(2-diethylamino-ethyl)-2-methoxy-benzamide

C₁₆H₁₆Cl₂NO₅P

O,O-dimethyl α-(2,3-dichlorophenoxyacetoxy)-3-nitrobenzylphosphonate

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