3-METHOXY-2'-METHYLBENZOPHENONE

Base Information

• Chemical Name: 3-METHOXY-2'-METHYLBENZOPHENONE
• CAS No.: 57800-65-4
• Molecular Formula: C15H14O2
• Molecular Weight: 226.27
• Hs Code.: 2914509090
• Mol file: 57800-65-4.mol

Synonyms:3-METHOXY-2'-METHYLBENZOPHENONE

Chemical Property of 3-METHOXY-2'-METHYLBENZOPHENONE

Chemical Property:

• Vapor Pressure: 8.8E-05mmHg at 25°C
• Boiling Point: 340.1°C at 760 mmHg
• Flash Point: 146.4°C
• PSA: 26.30000
• Density: 1.088g/cm³
• LogP: 3.23460

Purity/Quality:

97% ^*data from raw suppliers

3-Methoxy-2''-methylbenzophenone ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 3-METHOXY-2'-METHYLBENZOPHENONE

There total 3 articles about 3-METHOXY-2'-METHYLBENZOPHENONE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 41.0%

C15H16O2 (1223594-35-1,1269504-74-6,944672-22-4) → (3-methoxyphenyl)(o-tolyl)methanone (57800-65-4)

Guidance literature:

With sodium; In tetrahydrofuran; at 20 ℃; for 20h;

DOI:10.1016/j.tetlet.2009.11.079

Reference yield:

2-methylphenyl bromide (95-46-5) + 3-methoxy-benzaldehyde (591-31-1) → (3-methoxyphenyl)(o-tolyl)methanone (57800-65-4)

Guidance literature:

Multi-step reaction with 2 steps

1.1: magnesium; iodine

1.2: -40 - 20 °C / Schlenk technique; Inert atmosphere

2.1: pyridinium chlorochromate / dichloromethane / 20 °C

With iodine; magnesium; pyridinium chlorochromate; In dichloromethane;

DOI:10.1021/acs.orglett.6b00453

Reference yield:

3-methoxyphenyl bromide (2398-37-0) + ortho-toluoyl chloride (933-88-0) → (3-methoxyphenyl)(o-tolyl)methanone (57800-65-4)

Guidance literature:

With magnesium; Multistep reaction; 1.) THF, reflux, 2.) THF, from -20 deg C to RT;

DOI:10.1021/jm00059a015

upstream raw materials:

3-methoxyphenyl bromide

ortho-toluoyl chloride

C₁₅H₁₆O₂

2-methylphenyl bromide

Downstream raw materials:

(3-Hydroxy-phenyl)-o-tolyl-methanone

Acetic acid (2S,3R,4S,5R)-4,5-diacetoxy-2-[3-(2-methyl-benzoyl)-phenoxy]-tetrahydro-pyran-3-yl ester

o-Tolyl-[3-((2S,3R,4S,5R)-3,4,5-trihydroxy-tetrahydro-pyran-2-yloxy)-phenyl]-methanone

(R)-1-{2-[(E)-2-(3-Methoxy-phenyl)-2-o-tolyl-vinyloxy]-ethyl}-piperidine-3-carboxylic acid ethyl ester

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