3-Hexylthiophene-2-carbaldehyde

Base Information

Chemical Name:3-Hexylthiophene-2-carbaldehyde
CAS No.:222554-28-1
Molecular Formula:C11H16OS
Molecular Weight:196.313
Hs Code.:
DSSTox Substance ID:DTXSID40472146
Nikkaji Number:J3.493.503C
Wikidata:Q82300936
Mol file:222554-28-1.mol

Synonyms:3-hexylthiophene-2-carbaldehyde;222554-28-1;2-Thiophenecarboxaldehyde, 3-hexyl-;SCHEMBL820018;DTXSID40472146;3-Hexylthiophene-2-carboxaldehyde;MLMPDHSLKLLTJI-UHFFFAOYSA-N;ZB0866;s11879

Suppliers and Price of 3-Hexylthiophene-2-carbaldehyde

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 7 raw suppliers

Chemical Property of 3-Hexylthiophene-2-carbaldehyde

Chemical Property:

PSA：45.31000
LogP:3.68340
XLogP3:4.4
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:6
Exact Mass:196.09218630
Heavy Atom Count:13
Complexity:147

Purity/Quality:: 98%Min ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCCCCCC1=C(SC=C1)C=O

Technology Process of 3-Hexylthiophene-2-carbaldehyde

There total 3 articles about 3-Hexylthiophene-2-carbaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.6%

: 69249-61-2,125321-66-6
3-hexyl-2-bromothiophene

: 68-12-2,33513-42-7
N,N-dimethyl-formamide

: 222554-28-1
3-hexyl-2-thiophenecarboxaldehyde

Guidance literature:: 3-hexyl-2-bromothiophene; With n-butyllithium; In tetrahydrofuran; hexane; at -78 - -40 ℃; for 1h; Inert atmosphere;

N,N-dimethyl-formamide; In tetrahydrofuran; hexane; at -78 - 20 ℃;
DOI:10.1002/pola.24774

Reference yield: 92.0%

: 2591-86-8
N-Formylpiperidine

: 69249-61-2,125321-66-6
3-hexyl-2-bromothiophene

: 222554-28-1
3-hexyl-2-thiophenecarboxaldehyde

Guidance literature:: With n-butyllithium; In tetrahydrofuran; hexane; carbon dioxide;

Reference yield: 56.0%

: 1693-86-3
3-hexylthiophene

: 68-12-2,33513-42-7
N,N-dimethyl-formamide

: 222554-30-5
4-hexylthiophene-2-carbaldehyde

: 222554-28-1
3-hexyl-2-thiophenecarboxaldehyde

Guidance literature:: 3-hexylthiophene; With ethylmagnesium chloride; N-cyclohexyl-cyclohexanamine; In tetrahydrofuran; at 66 ℃; for 24h; Inert atmosphere;

N,N-dimethyl-formamide; In tetrahydrofuran; for 1h; regioselective reaction; Inert atmosphere;
DOI:10.1021/ja205953g