6H-Dibenz[b,d]azepin-6-one, 7-amino-5,7-dihydro-5-[(4-methoxyphenyl)methyl]-, hydrochloride (1:1)

Base Information

Chemical Name:6H-Dibenz[b,d]azepin-6-one, 7-amino-5,7-dihydro-5-[(4-methoxyphenyl)methyl]-, hydrochloride (1:1)
CAS No.:1083065-04-6
Molecular Formula:C22H21ClN2O2
Molecular Weight:380.874
Hs Code.:
Mol file:1083065-04-6.mol

Synonyms:6H-Dibenz[b,d]azepin-6-one, 7-amino-5,7-dihydro-5-[(4-methoxyphenyl)methyl]-, hydrochloride (1:1);7-amino-5-(4-methoxy-benzyl)-5H,7H-dibenzo[b,d]azepin-6-one hydrochloride

Suppliers and Price of 6H-Dibenz[b,d]azepin-6-one, 7-amino-5,7-dihydro-5-[(4-methoxyphenyl)methyl]-, hydrochloride (1:1)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
7-Amino-5,7-dihydro-5-[(4-methoxyphenyl)methyl]-6H-dibenz[b,d]azepin-6-oneHydrochloride
25mg
$ 430.00

TRC
7-Amino-5,7-dihydro-5-[(4-methoxyphenyl)methyl]-6H-dibenz[b,d]azepin-6-oneHydrochloride
10mg
$ 95.00

TRC
7-Amino-5,7-dihydro-5-[(4-methoxyphenyl)methyl]-6H-dibenz[b,d]azepin-6-oneHydrochloride
100mg
$ 1585.00

ChemScene
7-Amino-5-(4-methoxybenzyl)-5H-dibenzo[b,d]azepin-6(7H)-onehydrochloride 95.02%
500mg
$ 650.00

Total 3 raw suppliers

Chemical Property of 6H-Dibenz[b,d]azepin-6-one, 7-amino-5,7-dihydro-5-[(4-methoxyphenyl)methyl]-, hydrochloride (1:1)

Chemical Property:

PSA：55.56000
LogP:5.47610

Purity/Quality:

NLT 98% ^*data from raw suppliers

7-Amino-5,7-dihydro-5-[(4-methoxyphenyl)methyl]-6H-dibenz[b,d]azepin-6-oneHydrochloride ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 6H-Dibenz[b,d]azepin-6-one, 7-amino-5,7-dihydro-5-[(4-methoxyphenyl)methyl]-, hydrochloride (1:1)

There total 1 articles about 6H-Dibenz[b,d]azepin-6-one, 7-amino-5,7-dihydro-5-[(4-methoxyphenyl)methyl]-, hydrochloride (1:1) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 847926-87-8
5-(4-methoxybenzyl)-5H-dibenzo[b,d]azepine-6,7-dione-7-oxime

: 1083065-04-6
7-amino-5-(4-methoxy-benzyl)-5H,7H-dibenzo[b,d]azepin-6-one hydrochloride

Guidance literature:: With hydrogenchloride; palladium 10% on activated carbon; hydrogen; In methanol; water; at 50 ℃; for 48h; under 7500.75 Torr;

Reference yield: 42.4%

: 1083065-04-6
7-amino-5-(4-methoxy-benzyl)-5H,7H-dibenzo[b,d]azepin-6-one hydrochloride

: 14602-86-9,7635-53-2
(1R,2S,5R)-menthyl chloroformate

: 1083065-09-1
[(R)-5-(4-methoxy-benzyl)-6-oxo-6,7-dihydro-5H-dibenzo[b,d]azepin-7-yl]-carbamic acid (1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyl ester

: [(S)-5-(4-methoxy-benzyl)-6-oxo-6,7-dihydro-5H-dibenzo[b,d]azepin-7-yl]-carbamic acid (1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyl ester

Guidance literature:: With potassium carbonate; In tetrahydrofuran; water; at 20 - 40 ℃; for 1.41667h; optical yield given as %de; Large scale reaction;
DOI:10.1016/j.tetlet.2009.08.090