N2-BENZYL-N1,N1-DIETHYL-1,2-PROPANEDIAMINE

Base Information

• Chemical Name: N2-BENZYL-N1,N1-DIETHYL-1,2-PROPANEDIAMINE
• CAS No.: 108621-82-5
• Molecular Formula: C14H24N2
• Molecular Weight: 0
• Mol file: 108621-82-5.mol

Synonyms:N2-BENZYL-N1,N1-DIETHYL-1,2-PROPANEDIAMINE;N2-BENZYL-N1,N1-DIETHYLPROPANE-1,2-DIAMINE

Chemical Property of N2-BENZYL-N1,N1-DIETHYL-1,2-PROPANEDIAMINE

Chemical Property:

• Vapor Pressure: 0.000976mmHg at 25°C
• Boiling Point: 302.7°C at 760 mmHg
• Flash Point: 99.2°C
• PSA: 15.27000
• Density: 0.926g/cm³
• LogP: 2.89740

Purity/Quality:

BENZYL-[1-(DIETHYLAMINO)PROPAN-2-YL]AMINE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

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Technology Process of N2-BENZYL-N1,N1-DIETHYL-1,2-PROPANEDIAMINE

There total 3 articles about N2-BENZYL-N1,N1-DIETHYL-1,2-PROPANEDIAMINE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

1-benzyl-2-methylaziridine (24417-03-6) + N,N-diethyl(methylene)ammonium chloride (52853-18-6) → N-<2-Diaethylamino-1-methyl-aethyl>-benzylamin (108621-82-5)

Guidance literature:

In tetrahydrofuran; at 25 ℃; for 20h;

DOI:10.1055/s-2004-831174

Reference yield:

1-benzyl-2-methylaziridine (24417-03-6) + N,N-diethylmethyleneammonium ion (29344-13-6) → N-<2-Diaethylamino-1-methyl-aethyl>-benzylamin (108621-82-5)

Guidance literature:

1-benzyl-2-methylaziridine; With lithium iodide; In tetrahydrofuran; for 0.25h; Heating;

N,N-diethylmethyleneammonium ion; In tetrahydrofuran; at 25 ℃; for 20h;

With water; In tetrahydrofuran; diethyl ether;

DOI:10.1016/S0040-4039(03)01833-1

Reference yield:

→ N-<2-Diaethylamino-1-methyl-aethyl>-benzylamin (108621-82-5)

Guidance literature:

Benzylamin, 0.5 Mol 2-Chlor-1-diaethylamino-propan-hydrochlorid, 100grad, 12 h;

upstream raw materials:

1-benzyl-2-methylaziridine

N,N-diethylmethyleneammonium ion

N,N-diethyl(methylene)ammonium chloride

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