N-[(1R,2R)-1,2,3,4-TETRAHYDRO-1-HYDROXY-7-METHOXY-2-NAPHTHALENYL]-CHLOROACETAMIDE

Base Information

• Chemical Name: N-[(1R,2R)-1,2,3,4-TETRAHYDRO-1-HYDROXY-7-METHOXY-2-NAPHTHALENYL]-CHLOROACETAMIDE
• CAS No.: 153153-59-4
• Molecular Formula: C13H16ClNO3
• Molecular Weight: 269.72
• Mol file: 153153-59-4.mol

Synonyms:N-[(1R,2R)-1,2,3,4-TETRAHYDRO-1-HYDROXY-7-METHOXY-2-NAPHTHALENYL]-CHLOROACETAMIDE;(1R-trans)-2-Chloro-N-(1,2,3,4-tetrahydro-1-hydroxy-7-Methoxy-2-naphthalenyl)acetaMide

Chemical Property of N-[(1R,2R)-1,2,3,4-TETRAHYDRO-1-HYDROXY-7-METHOXY-2-NAPHTHALENYL]-CHLOROACETAMIDE

Chemical Property:

• Solubility.: Dichloromethane, Ethyl Acetate, Methanol

Purity/Quality:

96% ^*data from raw suppliers

N-[(1R,2R)-1,2,3,4-Tetrahydro-1-hydroxy-7-methoxy-2-naphthalenyl]chloroacetamide ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

• Uses: N-[(1R,2R)-1,2,3,4-Tetrahydro-1-hydroxy-7-methoxy-2-naphthalenyl]chloroacetamide (cas# 153153-59-4) is a compound useful in organic synthesis.

Technology Process of N-[(1R,2R)-1,2,3,4-TETRAHYDRO-1-HYDROXY-7-METHOXY-2-NAPHTHALENYL]-CHLOROACETAMIDE

There total 6 articles about N-[(1R,2R)-1,2,3,4-TETRAHYDRO-1-HYDROXY-7-METHOXY-2-NAPHTHALENYL]-CHLOROACETAMIDE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

trans-2-amino-7-methoxy-1,2,3,4-tetrahydronaphthalen-1-ol hydrochloride (2590-76-3,2590-78-5,91247-12-0) + chloroacetyl chloride (79-04-9) → trans-2-(chloroacetylamino)-7-methoxy-1-tetralol (92421-91-5,153153-59-4,99833-89-3)

Guidance literature:

With sodium hydroxide; In dichloromethane; water; for 2h; Ambient temperature;

Reference yield: 60.0%

2-Chloro-N-(7-methoxy-1-oxo-1,2,3,4-tetrahydro-naphthalen-2-yl)-acetamide (92421-83-5) → trans-2-(chloroacetylamino)-7-methoxy-1-tetralol (92421-91-5,153153-59-4,99833-89-3)

Guidance literature:

With sodium tetrahydroborate; In ethanol;

DOI:10.1021/jm00378a014

Reference yield: 40.0%

(1RS,2RS)-2-amino-1,2,3,4-tetrahydro-7-methoxy-1-naphthol (131073-43-3) + chloroacetyl chloride (79-04-9) → trans-2-(chloroacetylamino)-7-methoxy-1-tetralol (92421-91-5,153153-59-4,99833-89-3)

Guidance literature:

With sodium hydroxide; In dichloromethane; water; for 4h; Ambient temperature;

upstream raw materials:

(1RS,2RS)-2-amino-1,2,3,4-tetrahydro-7-methoxy-1-naphthol

chloroacetyl chloride

trans-2-amino-7-methoxy-1,2,3,4-tetrahydronaphthalen-1-ol hydrochloride

2-Chloro-N-(7-methoxy-1-oxo-1,2,3,4-tetrahydro-naphthalen-2-yl)-acetamide

Downstream raw materials:

trans-9-methoxy-2,3,4a,5,6,10b-hexahydro-4H-naphth<1,2-b><1,4>oxazin-3-one

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