2,3-Dichloro-6-methyl-4-nitroaniline

Base Information

• Chemical Name: 2,3-Dichloro-6-methyl-4-nitroaniline
• CAS No.: 13852-56-7
• Molecular Formula: C₇H₆Cl₂N₂O₂
• Molecular Weight: 221.043
• DSSTox Substance ID: DTXSID90702763
• Nikkaji Number: J81.688D
• Wikidata: Q82634762
• Mol file: 13852-56-7.mol

Synonyms:2,3-Dichloro-6-methyl-4-nitroaniline;13852-56-7;DTXSID90702763

Chemical Property of 2,3-Dichloro-6-methyl-4-nitroaniline

Chemical Property:

• XLogP3: 2.7
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 0
• Exact Mass: 219.9806328
• Heavy Atom Count: 13
• Complexity: 209

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC1=CC(=C(C(=C1N)Cl)Cl)[N+](=O)[O-]

Technology Process of 2,3-Dichloro-6-methyl-4-nitroaniline

There total 1 articles about 2,3-Dichloro-6-methyl-4-nitroaniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N-(5-chloro-2-methyl-4-nitrophenyl)acetamide (13852-50-1) → 5,6-Dichlor-4-nitro-2-methyl-anilin (13852-56-7)

Guidance literature:

Multistep reaction; (i) Cl₂, AsCl₃, (ii) aq. H₂SO₄;

DOI:10.1039/j39670000400

Reference yield:

5,6-Dichlor-4-nitro-2-methyl-anilin (13852-56-7) → 1,2-Dichlor-3,6-diamino-5-methyl-benzol (13711-11-0)

Guidance literature:

With hydrogen; platinum on activated charcoal;

DOI:10.1039/j39670000400

Reference yield:

5,6-Dichlor-4-nitro-2-methyl-anilin (13852-56-7) → 1,2-dichloro-5-methyl-3-nitrobenzene (13711-25-6)

Guidance literature:

Multistep reaction; (i) NaNO₂, H₂SO₄, (ii) Cu;

DOI:10.1039/j39670000400

upstream raw materials:

N-(5-chloro-2-methyl-4-nitrophenyl)acetamide

Downstream raw materials:

1,2-Dichlor-3-N-ethylamino-5-methyl-benzol

1,2-Dichlor-3,6-diamino-5-methyl-benzol

1,2-dichloro-5-methyl-3-nitrobenzene

2,3-dichloro-5-methylphenylamine