7-BroMo-1,2,3,3a,4,8b-hexahydro-4-(4-Methylphenyl)cyclopent[b]indole

Base Information

Chemical Name:7-BroMo-1,2,3,3a,4,8b-hexahydro-4-(4-Methylphenyl)cyclopent[b]indole
CAS No.:1250863-85-4
Molecular Formula:C18H18BrN
Molecular Weight:328.252
Hs Code.:
Mol file:1250863-85-4.mol

Synonyms:7-BroMo-1,2,3,3a,4,8b-hexahydro-4-(4-Methylphenyl)cyclopent[b]indole

Suppliers and Price of 7-BroMo-1,2,3,3a,4,8b-hexahydro-4-(4-Methylphenyl)cyclopent[b]indole

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
7-Bromo-?1,?2,?3,?3a,?4,?8b-?hexahydro-?4-?(4-?methylphenyl)?cyclopent[b]?indole
50mg
$ 165.00

Total 3 raw suppliers

Chemical Property of 7-BroMo-1,2,3,3a,4,8b-hexahydro-4-(4-Methylphenyl)cyclopent[b]indole

Chemical Property:

PSA：3.24000
LogP:5.61030

Purity/Quality:

97% ^*data from raw suppliers

7-Bromo-?1,?2,?3,?3a,?4,?8b-?hexahydro-?4-?(4-?methylphenyl)?cyclopent[b]?indole ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Uses 7-Bromo-1,2,3,3a,4,8b-hexahydro-4-(4-methylphenyl)cyclopent[b]indole is used in the synthesis of dye sensitized solar cells constituted of chromophores.

Technology Process of 7-BroMo-1,2,3,3a,4,8b-hexahydro-4-(4-Methylphenyl)cyclopent[b]indole

There total 2 articles about 7-BroMo-1,2,3,3a,4,8b-hexahydro-4-(4-Methylphenyl)cyclopent[b]indole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 273220-33-0
4-(p-tolyl)-1,2,3,3a,4,8b-hexahydrocyclopenta[b]indole

: 1250863-85-4
7-bromo-1,2,3,3a,4,8b-hexahydro-4-(4-methylphenyl)-cyclopent-[b]indole

Guidance literature:: With N-Bromosuccinimide; In acetone; for 2h; Inert atmosphere;

Reference yield:

: 80278-94-0
1,2,3,3a,4,8b-hexahydrocyclopent[b]indole

: 1250863-85-4
7-bromo-1,2,3,3a,4,8b-hexahydro-4-(4-methylphenyl)-cyclopent-[b]indole

Guidance literature:: Multi-step reaction with 2 steps

1: palladium diacetate; johnphos; sodium t-butanolate / toluene / Reflux

2: N-Bromosuccinimide / acetone / 5 h / 20 °C / Inert atmosphere

With N-Bromosuccinimide; palladium diacetate; johnphos; sodium t-butanolate; In acetone; toluene;
DOI:10.1039/c2jm30978e

Reference yield: 60.0%

: 850881-09-3
3-hexylthiophene-2-boronic acid pinacol ester

: 1250863-85-4
7-bromo-1,2,3,3a,4,8b-hexahydro-4-(4-methylphenyl)-cyclopent-[b]indole

: 7-(3-hexylthiophen-2-yl)

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate; In tetrahydrofuran; for 12h; Inert atmosphere; Reflux;
DOI:10.1016/j.tet.2016.10.057