methyl 4-chloro-5-iodo-2-(2-(phenylsulfonyl)acetamido)benzoate

Base Information

Chemical Name:methyl 4-chloro-5-iodo-2-(2-(phenylsulfonyl)acetamido)benzoate
CAS No.:1398338-67-4
Molecular Formula:C₁₆H₁₃ClINO₅S
Molecular Weight:493.706
Hs Code.:
Mol file:1398338-67-4.mol

Synonyms:methyl 4-chloro-5-iodo-2-(2-(phenylsulfonyl)acetamido)benzoate

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Chemical Property of methyl 4-chloro-5-iodo-2-(2-(phenylsulfonyl)acetamido)benzoate

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Technology Process of methyl 4-chloro-5-iodo-2-(2-(phenylsulfonyl)acetamido)benzoate

There total 2 articles about methyl 4-chloro-5-iodo-2-(2-(phenylsulfonyl)acetamido)benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.4%

: 3959-23-7
benzenesulfonylacetic acid

: 199850-56-1
methyl 2-amino-4-chloro-5-iodobenzoate

: 1398338-67-4
methyl 4-chloro-5-iodo-2-(2-(phenylsulfonyl)acetamido)benzoate

Guidance literature:: benzenesulfonylacetic acid; With oxalyl dichloride; N,N-dimethyl-formamide; In dichloromethane; at 20 ℃; for 2h;

methyl 2-amino-4-chloro-5-iodobenzoate; With triethylamine; In dichloromethane; at 20 ℃;

With sodium hydrogencarbonate; In dichloromethane; water;

Reference yield:

: 5900-58-3
2-amino-4-chloro-benzoic acid methyl ester

: 1398338-67-4
methyl 4-chloro-5-iodo-2-(2-(phenylsulfonyl)acetamido)benzoate

Guidance literature:: Multi-step reaction with 2 steps

1.1: iodine; silver sulfate / ethanol

2.1: oxalyl dichloride / N,N-dimethyl-formamide / dichloromethane / 2 h / 20 °C

2.2: 20 °C

With oxalyl dichloride; iodine; silver sulfate; N,N-dimethyl-formamide; In ethanol; dichloromethane;