2-Furfurylidene-3,4,4a,5,6,7,8,8aβ-octahydronaphthalen-1(2H)-one

Base Information

• Chemical Name: 2-Furfurylidene-3,4,4a,5,6,7,8,8aβ-octahydronaphthalen-1(2H)-one
• CAS No.: 17429-47-9
• Molecular Formula: C₁₅H₁₈O₂
• Molecular Weight: 230.307
• Mol file: 17429-47-9.mol

Synonyms:2-Furfurylidene-3,4,4a,5,6,7,8,8aβ-octahydronaphthalen-1(2H)-one

Chemical Property of 2-Furfurylidene-3,4,4a,5,6,7,8,8aβ-octahydronaphthalen-1(2H)-one

Chemical Property:

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2-Furfurylidene-3,4,4a,5,6,7,8,8aβ-octahydronaphthalen-1(2H)-one

There total 1 articles about 2-Furfurylidene-3,4,4a,5,6,7,8,8aβ-octahydronaphthalen-1(2H)-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

furfural (98-01-1) + trans-1-decalone (21370-71-8) → (+/-)-2-((Ξ)-furfuryliden)-(4ar,8at)-octahydro-naphthalen-1-one (17429-47-9,58822-81-4)

Guidance literature:

With sodium hydroxide;

DOI:10.1021/ja01605a016

Reference yield:

(+/-)-2-((Ξ)-furfuryliden)-(4ar,8at)-octahydro-naphthalen-1-one (17429-47-9,58822-81-4) → (+/-)-3-(2c-carboxy-2t-methyl-cyclohex-r-yl)-propionic acid (91966-67-5)

Guidance literature:

Multi-step reaction with 2 steps

1: potassium tert-butylate; tert-butyl alcohol

2: ozone; ethyl acetate / anschliessend mit wss. H₂O₂ in Essigsaeure und wss. HCl behandeln

With potassium tert-butylate; ozone; ethyl acetate; tert-butyl alcohol;

DOI:10.1021/ja01605a016

Reference yield:

(+/-)-2-((Ξ)-furfuryliden)-(4ar,8at)-octahydro-naphthalen-1-one (17429-47-9,58822-81-4) + methyl iodide (74-88-4) → (+/-)-2-((Ξ)-furfurylidene)-8a-methyl-(4ar,8at)-octahydro-naphthalen-1-one (54482-61-0,56051-40-2,56192-67-7) + (+/-)-2-((Ξ)-furfurylidene)8a-methyl-(4ar,8ac)-octahydro-naphthalen-1-one (54482-61-0,56051-40-2,56192-67-7)

Guidance literature:

With potassium tert-butylate; tert-butyl alcohol;

DOI:10.1021/ja01605a016

upstream raw materials:

furfural

trans-1-decalone

Downstream raw materials:

(+/-)-2-((Ξ)-furfurylidene)-8a-methyl-(4ar,8at)-octahydro-naphthalen-1-one

(+/-)-2-((Ξ)-furfurylidene)8a-methyl-(4ar,8ac)-octahydro-naphthalen-1-one

3-[2t-(2-cyano-propyl)-2c-formyl-cyclohex-r-yl]-propionic acid

(+/-)-3-(2c-carboxy-2t-methyl-cyclohex-r-yl)-propionic acid