N1,N1-Bis(4-aMinophenyl)benzene-1,4-diaMine trihydrochloride

Base Information

• Chemical Name: N1,N1-Bis(4-aMinophenyl)benzene-1,4-diaMine trihydrochloride
• CAS No.: 114254-48-7
• Molecular Formula: C₁₈H₁₈N₄*3ClH
• Molecular Weight: 399.751
• Mol file: 114254-48-7.mol

Synonyms:N1,N1-Bis(4-aMinophenyl)benzene-1,4-diaMine trihydrochloride;N1,N1-bis(4-aMinophenyl)benzene-1,4-diaMine;tris(4-amino)phenylamine trihydrochloride

Chemical Property of N1,N1-Bis(4-aMinophenyl)benzene-1,4-diaMine trihydrochloride

Chemical Property:

• PSA: 81.30000
• LogP: 8.05260
• Storage Temp.: Sealed in dry,Room Temperature

Purity/Quality:

97% ^*data from raw suppliers

N1,N1-Bis(4-aminophenyl)benzene-1,4-diamine trihydrochloride 95+% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of N1,N1-Bis(4-aMinophenyl)benzene-1,4-diaMine trihydrochloride

There total 3 articles about N1,N1-Bis(4-aMinophenyl)benzene-1,4-diaMine trihydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-nitro-aniline (100-01-6,104810-17-5) → tris(4-amino)phenylamine trihydrochloride (114254-48-7)

Guidance literature:

Multi-step reaction with 2 steps

1: K₂CO₃; Cu / dimethylformamide / 48 h / Heating

2: SnCl₂; HCl / 5 h / Heating

With hydrogenchloride; copper; potassium carbonate; tin(ll) chloride; In N,N-dimethyl-formamide;

DOI:10.1246/bcsj.78.1362

Reference yield:

4-chlorobenzonitrile (100-00-5) → tris(4-amino)phenylamine trihydrochloride (114254-48-7)

Guidance literature:

Multi-step reaction with 2 steps

1: K₂CO₃; Cu / dimethylformamide / 48 h / Heating

2: SnCl₂; HCl / 5 h / Heating

With hydrogenchloride; copper; potassium carbonate; tin(ll) chloride; In N,N-dimethyl-formamide;

DOI:10.1246/bcsj.78.1362

Reference yield:

tris(4-nitrophenyl)amine (20440-93-1) → tris(4-amino)phenylamine trihydrochloride (114254-48-7)

Guidance literature:

With hydrogenchloride; tin(ll) chloride; for 5h; Heating;

DOI:10.1246/bcsj.78.1362

upstream raw materials:

tris(4-nitrophenyl)amine

4-nitro-aniline

4-chlorobenzonitrile