(S)-7-AMino-5-Methyl-5,7-dihydro-6H-dibenzo[b,d]azepin-6-one Hydrochloride

Base Information

• Chemical Name: (S)-7-AMino-5-Methyl-5,7-dihydro-6H-dibenzo[b,d]azepin-6-one Hydrochloride
• CAS No.: 209984-55-4
• Molecular Formula: C₁₅H₁₄N₂O*ClH
• Molecular Weight: 274.75
• Hs Code.: 2933990090
• Mol file: 209984-55-4.mol

Synonyms:(S)-7-AMino-5-Methyl-5,7-dihydro-6H-dibenzo[b,d]azepin-6-one Hydrochloride;6H-Dibenz[b,d]azepin-6-one, 7-aMino-5,7-dihydro-5-Methyl- (hydrochloride)(1:1),(7S)-;(S)-7-Amino-5-methyl-5,7-dihydro-6h-dibenzo[b,d]azepin-6-one HCl

Chemical Property of (S)-7-AMino-5-Methyl-5,7-dihydro-6H-dibenzo[b,d]azepin-6-one Hydrochloride

Chemical Property:

• PSA: 46.33000
• LogP: 3.89710
• Storage Temp.: Sealed in dry,Room Temperature

Purity/Quality:

97% ^*data from raw suppliers

(S)-7-Amino-5-methyl-5,7-dihydro-6H-dibenzo[b,d]azepin-6-one hydrochloride ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of (S)-7-AMino-5-Methyl-5,7-dihydro-6H-dibenzo[b,d]azepin-6-one Hydrochloride

There total 2 articles about (S)-7-AMino-5-Methyl-5,7-dihydro-6H-dibenzo[b,d]azepin-6-one Hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

(S,S)-7-amino-5-methyl-5H-dibenzo[b,d]azepin-6(7H)-one (2S,3S)-2,3-bis(4-methylbenzoyloxy)succinate → (S,S)-7-amino-5-methyl-5H-dibenzo[b,d]azepin-6(7H)-one hydrochloride (209984-55-4,209984-32-7)

Guidance literature:

With hydrogenchloride; In ethanol; water; at 50 ℃;

DOI:10.1016/j.tetasy.2009.04.016

Reference yield:

7-amino-5-methyl-5H-dibenzo[b,d]azepin-6(7H)-one hydrochloride (213024-76-1) → (S,S)-7-amino-5-methyl-5H-dibenzo[b,d]azepin-6(7H)-one hydrochloride (209984-55-4,209984-32-7)

Guidance literature:

7-amino-5-methyl-5H-dibenzo[b,d]azepin-6(7H)-one hydrochloride; With (2S,3S)-di-4-toluoyltartaric acid; In methanol; at 20 ℃; for 8 - 72h;

With sodium hydrogencarbonate; In ethyl acetate; pH=9 - 10;

With hydrogenchloride; In methanol;

upstream raw materials:

7-amino-5-methyl-5H-dibenzo[b,d]azepin-6(7H)-one hydrochloride