Ethyl 1-(3,4-dichlorobenzyl)-4-nitro-1H-indole-2-carboxylate

Base Information

• Chemical Name: Ethyl 1-(3,4-dichlorobenzyl)-4-nitro-1H-indole-2-carboxylate
• CAS No.: 220677-29-2
• Molecular Formula: C₁₈H₁₄Cl₂N₂O₄
• Molecular Weight: 393.226
• Mol file: 220677-29-2.mol

Synonyms:Ethyl 1-(3,4-dichlorobenzyl)-4-nitro-1H-indole-2-carboxylate

Chemical Property of Ethyl 1-(3,4-dichlorobenzyl)-4-nitro-1H-indole-2-carboxylate

Chemical Property:

Purity/Quality:

95+% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
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MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Ethyl 1-(3,4-dichlorobenzyl)-4-nitro-1H-indole-2-carboxylate

There total 4 articles about Ethyl 1-(3,4-dichlorobenzyl)-4-nitro-1H-indole-2-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

2-Methylpentane (107-83-5) + 4-nitro-1H-indole-2-carboxylic acid ethyl ester (4993-93-5) + 3,4-Dichlorophenylmethyl chloride (102-47-6) → Ethyl N-(3,4-dichlorobenzyl)-4-nitroindole-2-carboxylate (220677-29-2)

Guidance literature:

With potassium iodide; potassium carbonate; In N,N-dimethyl-formamide;

Reference yield: 78.0%

2-Methylpentane (107-83-5) + 4-nitro-1H-indole-2-carboxylic acid ethyl ester (4993-93-5) + tetra(n-butyl)ammonium hydrogensulfate (32503-27-8) + 3,4-Dichlorophenylmethyl chloride (102-47-6) → Ethyl N-(3,4-dichlorobenzyl)-4-nitroindole-2-carboxylate (220677-29-2)

Guidance literature:

With sodium hydroxide; In dichloromethane;

Reference yield: 69.0%

→ Ethyl N-(3,4-dichlorobenzyl)-4-nitroindole-2-carboxylate (220677-29-2)

Guidance literature:

upstream raw materials:

4-nitro-1H-indole-2-carboxylic acid ethyl ester

3,4-Dichlorophenylmethyl chloride

2-Methylpentane

tetra(n-butyl)ammonium hydrogensulfate

Downstream raw materials:

ethyl N-(3,4-dichlorobenzyl)-4-aminoindole-2-carboxylate

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