3-(3-hydroxyphenyl)-1-Pyrrolidinecarboxylic acid 1,1-diMethylethyl ester

Base Information

Chemical Name:3-(3-hydroxyphenyl)-1-Pyrrolidinecarboxylic acid 1,1-diMethylethyl ester
CAS No.:1094217-59-0
Molecular Formula:C₁₅H₂₁NO₃
Molecular Weight:263.337
Hs Code.:
Mol file:1094217-59-0.mol

Synonyms:3-(3-hydroxyphenyl)-1-Pyrrolidinecarboxylic acid 1,1-diMethylethyl ester

Suppliers and Price of 3-(3-hydroxyphenyl)-1-Pyrrolidinecarboxylic acid 1,1-diMethylethyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Crysdot
tert-Butyl3-(3-hydroxyphenyl)pyrrolidine-1-carboxylate 95+%
1g
$ 920.00

Chemenu
tert-Butyl3-(3-hydroxyphenyl)pyrrolidine-1-carboxylate 95%
1g
$ 720.00

Alichem
tert-Butyl3-(3-hydroxyphenyl)pyrrolidine-1-carboxylate
1g
$ 930.60

AK Scientific
3-(3-HYDROXYPHENYL)-1-PYRROLIDINECARBOXYLICACID1,1-DIMETHYLETHYLESTER
1g
$ 1808.00

Total 5 raw suppliers

Chemical Property of 3-(3-hydroxyphenyl)-1-Pyrrolidinecarboxylic acid 1,1-diMethylethyl ester

Chemical Property:

Storage Temp.:2-8°C

Purity/Quality:

97% ^*data from raw suppliers

tert-Butyl3-(3-hydroxyphenyl)pyrrolidine-1-carboxylate 95+% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 3-(3-hydroxyphenyl)-1-Pyrrolidinecarboxylic acid 1,1-diMethylethyl ester

There total 6 articles about 3-(3-hydroxyphenyl)-1-Pyrrolidinecarboxylic acid 1,1-diMethylethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 1-tert-butoxycarbonyl-3-(3-hydroxyphenyl)-2,5-dihydro-1H-pyrrolidine

: 1094217-59-0
1-tert-butoxycarbonyl-3-(3-hydroxyphenyl)pyrrolidine

Guidance literature:: With palladium on activated charcoal; hydrogen; In methanol; at 20 ℃; for 3h; under 760.051 Torr;

Reference yield:

: 630121-86-7
3-(((trifluoromethyl)sulfonyl)oxy)-2,5-dihydro-1H-pyrrole-1-carboxylic acid tert-butyl ester

: 1094217-59-0
1-tert-butoxycarbonyl-3-(3-hydroxyphenyl)pyrrolidine

Guidance literature:: Multi-step reaction with 3 steps

1: potassium acetate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / 1,4-dioxane / 5 h / 95 °C / Inert atmosphere

2: potassium carbonate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / N,N-dimethyl-formamide / 16 h

3: hydrogen; palladium on activated charcoal / methanol / 3 h / 20 °C / 760.05 Torr

With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; palladium on activated charcoal; hydrogen; potassium acetate; potassium carbonate; In 1,4-dioxane; methanol; N,N-dimethyl-formamide;

Reference yield:

: 212127-83-8
tert-butyl 3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-2,5-dihydropyrrole-1-carboxylate

: 1094217-59-0
1-tert-butoxycarbonyl-3-(3-hydroxyphenyl)pyrrolidine

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / N,N-dimethyl-formamide / 16 h

2: hydrogen; palladium on activated charcoal / methanol / 3 h / 20 °C / 760.05 Torr

With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; palladium on activated charcoal; hydrogen; potassium carbonate; In methanol; N,N-dimethyl-formamide;