AcetaMide, 2,2,2-trichloro-N-[2-(trifluoroMethyl)phenyl]-

Base Information

Chemical Name:AcetaMide, 2,2,2-trichloro-N-[2-(trifluoroMethyl)phenyl]-
CAS No.:349416-85-9
Molecular Formula:C9H5Cl3F3NO
Molecular Weight:306.4963096
Hs Code.:
Mol file:349416-85-9.mol

Synonyms:AcetaMide, 2,2,2-trichloro-N-[2-(trifluoroMethyl)phenyl]-

Suppliers and Price of AcetaMide, 2,2,2-trichloro-N-[2-(trifluoroMethyl)phenyl]-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
2,2,2-TRICHLORO-N-[2-(TRIFLUOROMETHYL)PHENYL]ACETAMIDE 95.00%
5MG
$ 497.18

Total 5 raw suppliers

Chemical Property of AcetaMide, 2,2,2-trichloro-N-[2-(trifluoroMethyl)phenyl]-

Chemical Property:

Melting Point:46 °C
PSA：29.10000
LogP:4.08710

Purity/Quality:

98%min ^*data from raw suppliers

2,2,2-TRICHLORO-N-[2-(TRIFLUOROMETHYL)PHENYL]ACETAMIDE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of AcetaMide, 2,2,2-trichloro-N-[2-(trifluoroMethyl)phenyl]-

There total 1 articles about AcetaMide, 2,2,2-trichloro-N-[2-(trifluoroMethyl)phenyl]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 76-02-8
trifluoroacetyl chloride

: 88-17-5
2-(trifluoromethyl)benzenamine

: 349416-85-9
2,2,2-trichloro-N-(2-(trifluoromethyl)phenyl)acetamide

Guidance literature:: In 1,4-dioxane; for 0.5h; Cooling with ice;
DOI:10.1080/07328301003597673

Reference yield: 33.0%

: 349416-85-9
2,2,2-trichloro-N-(2-(trifluoromethyl)phenyl)acetamide

: 1228763-36-7
N-(2-trifluoromethylphenyl)dichloroacetimidoyl chloride

Guidance literature:: With triphenylphosphine; In tetrachloromethane; dichloromethane; at 60 ℃; for 4h;
DOI:10.1080/07328301003597673

Reference yield:

: 349416-85-9
2,2,2-trichloro-N-(2-(trifluoromethyl)phenyl)acetamide

: 1228757-53-6
N-(2-trifluoromethylphenyl)-O-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl) dichloroacetimidate

: N-(2-trifluoromethylphenyl)-O-(2,3,4,6-tetra-O-acetyl-α-D-glucopyranosyl) dichloroacetimidate

Guidance literature:: Multi-step reaction with 2 steps

1.1: triphenylphosphine / tetrachloromethane; dichloromethane / 4 h / 60 °C

2.1: 15-crown-5; sodium hydride / dichloromethane / 0.08 h / 20 °C / Inert atmosphere

2.2: 0.5 h / 20 °C / Inert atmosphere

With 15-crown-5; sodium hydride; triphenylphosphine; In tetrachloromethane; dichloromethane;
DOI:10.1080/07328301003597673