2,3-Bis(dimethylamino)acrylaldehyde

Base Information

• Chemical Name: 2,3-Bis(dimethylamino)acrylaldehyde
• CAS No.: 42145-18-6
• Molecular Formula: C₇H₁₄N₂O
• Molecular Weight: 142.201
• Mol file: 42145-18-6.mol

Synonyms:2,3-Bis(dimethylamino)acrylaldehyde;2,3-Bis(dimethylamino)propenal

Chemical Property of 2,3-Bis(dimethylamino)acrylaldehyde

Chemical Property:

• Boiling Point: 65 - 67 °C (0.3 mmHg)
• PSA: 23.55000
• LogP: 0.14990

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2,3-Bis(dimethylamino)acrylaldehyde

There total 6 articles about 2,3-Bis(dimethylamino)acrylaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

bis 1,2-(dimethylamino)ethylene (19289-58-8) + N,N-dimethyl-formamide (68-12-2,33513-42-7) → 1,2-Bis-(dimethylamino)acrylaldehyd (42145-18-6) + C9H20N3(1+)*ClO4(1-)

Guidance literature:

With trichlorophosphate;

DOI:10.1007/BF00962665

Reference yield:

C9H20N3(1+)*ClO4(1-) → 1,2-Bis-(dimethylamino)acrylaldehyd (42145-18-6)

Guidance literature:

With potassium carbonate; In benzene;

Reference yield:

((Z)-2,3-Bis-dimethylamino-allylidene)-dimethyl-ammonium; chloride → 2,3-Bis(dimethylamino)acrolein (42145-18-6)

Guidance literature:

With water; potassium carbonate; at 70 ℃; for 2h; Yield given;

upstream raw materials:

bis 1,2-(dimethylamino)ethylene

N,N-dimethyl-formamide

dimethylamino-propynal

dimethyl amine

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