(2R,3S)-2,3,4-Trihydroxy-γ-butyrolactone 2,3-Cyclohexyl Ketal

Base Information

Chemical Name:(2R,3S)-2,3,4-Trihydroxy-γ-butyrolactone 2,3-Cyclohexyl Ketal
CAS No.:186803-48-5
Molecular Formula:C₁₀H₁₄O₅
Molecular Weight:214.218
Hs Code.:
Mol file:186803-48-5.mol

Synonyms:(2R,3S)-2,3,4-Trihydroxy-γ-butyrolactone 2,3-Cyclohexyl Ketal;(3'aR,6'aS)-Dihydro-6'-hydroxy-spiro[cyclohexane-1,2'-furo[3,4-d][1,3]dioxol]-4'(3'aH)-one

Suppliers and Price of (2R,3S)-2,3,4-Trihydroxy-γ-butyrolactone 2,3-Cyclohexyl Ketal

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
(2R,3S)-2,3,4-Trihydroxy-γ-butyrolactone2,3-CyclohexylKetal
500mg
$ 475.00

Total 9 raw suppliers

Chemical Property of (2R,3S)-2,3,4-Trihydroxy-γ-butyrolactone 2,3-Cyclohexyl Ketal

Chemical Property:

PSA：64.99000
LogP:0.30600
Storage Temp.:Refrigerator
Solubility.:Chloroform, DMSO, Methanol

Purity/Quality:

99% ^*data from raw suppliers

(2R,3S)-2,3,4-Trihydroxy-γ-butyrolactone2,3-CyclohexylKetal ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of (2R,3S)-2,3,4-Trihydroxy-γ-butyrolactone 2,3-Cyclohexyl Ketal

There total 4 articles about (2R,3S)-2,3,4-Trihydroxy-γ-butyrolactone 2,3-Cyclohexyl Ketal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 27304-20-7,546141-19-9
2,3-O-cyclohexylidene-γ-D-ribonolactone

: 186803-48-5
2,3-O-cyclohexylidene-L-(-)-erythruronic acid

Guidance literature:: With sodium hydroxide; sodium periodate; In 1,4-dioxane; at 0 ℃; for 0.166667h;
DOI:10.1055/s-1991-26609

Reference yield:

: 108-94-1,11119-77-0,9003-41-2,9075-99-4
cyclohexanone

: 186803-48-5
2,3-O-cyclohexylidene-L-(-)-erythruronic acid

Guidance literature:: Multi-step reaction with 3 steps

1: 82 percent / conc. H₂SO₄ / 2 h / Ambient temperature

2: 59 percent / pyridinium chlorochromate / CH₂Cl₂ / 16 h / Ambient temperature; or with pyridinium dichromate

3: 96 percent / aq. NaOH, aq. NaIO₄ / dioxane / 0.17 h / 0 °C

With sodium hydroxide; sodium periodate; sulfuric acid; pyridinium chlorochromate; In 1,4-dioxane; dichloromethane;
DOI:10.1055/s-1991-26609

Reference yield:

: 123168-27-4
2,3-O-cyclohexylidene-D-ribofuranose

: 186803-48-5
2,3-O-cyclohexylidene-L-(-)-erythruronic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 59 percent / pyridinium chlorochromate / CH₂Cl₂ / 16 h / Ambient temperature; or with pyridinium dichromate

2: 96 percent / aq. NaOH, aq. NaIO₄ / dioxane / 0.17 h / 0 °C

With sodium hydroxide; sodium periodate; pyridinium chlorochromate; In 1,4-dioxane; dichloromethane;
DOI:10.1055/s-1991-26609