2H,5H,7H-4a,8:6,10-Dimethanopyridazino(4,3-e)(1,3)diazocine-10(9H)-acetic acid, 3,4-dihydro-3-oxo-, hydrazine

Base Information

Chemical Name:2H,5H,7H-4a,8:6,10-Dimethanopyridazino(4,3-e)(1,3)diazocine-10(9H)-acetic acid, 3,4-dihydro-3-oxo-, hydrazine
CAS No.:172984-93-9
Molecular Formula:C₁₂H₁₈N₆O₂
Molecular Weight:278.314
Hs Code.:
DSSTox Substance ID:DTXSID10169455

Synonyms:172984-93-9;2H,5H,7H-4a,8:6,10-Dimethanopyridazino(4,3-e)(1,3)diazocine-10(9H)-acetic acid, 3,4-dihydro-3-oxo-, hydrazine;DTXSID10169455;LS-62022

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2H,5H,7H-4a,8:6,10-Dimethanopyridazino(4,3-e)(1,3)diazocine-10(9H)-acetic acid, 3,4-dihydro-3-oxo-, hydrazine

Chemical Property:

Boiling Point:°Cat760mmHg
Flash Point:°C
Density:1.86g/cm³
XLogP3:-3.1
Hydrogen Bond Donor Count:3
Hydrogen Bond Acceptor Count:6
Rotatable Bond Count:2
Exact Mass:278.14912384
Heavy Atom Count:20
Complexity:516

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C1C(=O)NN=C2C13CN4CC2(CN(C3)C4)CC(=O)NN

Technology Process of 2H,5H,7H-4a,8:6,10-Dimethanopyridazino(4,3-e)(1,3)diazocine-10(9H)-acetic acid, 3,4-dihydro-3-oxo-, hydrazine

There total 5 articles about 2H,5H,7H-4a,8:6,10-Dimethanopyridazino(4,3-e)(1,3)diazocine-10(9H)-acetic acid, 3,4-dihydro-3-oxo-, hydrazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.8%

: 172984-91-7
5,7-di(ethoxycarbonylmethyl)-6-oxo-1,3-diazaadamantane

: 172984-93-9
10-hydrazinocarbonylmethyl-4a,8:6,10-dimethano-4,4a,5,6,7,8,9,10-octahydropyridazino<4,3-e><1,3>diazocin-3(2H)-one

Guidance literature:: With hydrazine hydrate; In ethanol; for 5h; Heating;
DOI:10.1007/BF02219065

Reference yield: 54.7%

: 5,7-di(isopropoxycarbonylmethyl)-6-oxo-1,3-diazaadamantane

: 172984-93-9
10-hydrazinocarbonylmethyl-4a,8:6,10-dimethano-4,4a,5,6,7,8,9,10-octahydropyridazino<4,3-e><1,3>diazocin-3(2H)-one

Guidance literature:: With hydrazine hydrate; In ethanol; for 5h; Heating;
DOI:10.1007/BF02219065

Reference yield:

: 100-97-0
hexamethylenetetramine

: 172984-93-9
10-hydrazinocarbonylmethyl-4a,8:6,10-dimethano-4,4a,5,6,7,8,9,10-octahydropyridazino<4,3-e><1,3>diazocin-3(2H)-one

Guidance literature:: Multi-step reaction with 2 steps

1: 16 percent / AcOH / butan-1-ol / 10 h / Heating

2: 62.8 percent / hydrazine hydrate / ethanol / 5 h / Heating

With hydrazine hydrate; acetic acid; In ethanol; butan-1-ol;
DOI:10.1007/BF02219065