Technology Process of 4,8-Dioxo-2-adamantanecarboxylic acid
There total 10 articles about 4,8-Dioxo-2-adamantanecarboxylic acid which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1: p-toluenesulfonic acid / benzene / 2 h / Heating
2: 2.) 10percent aq. HCl / 1.) CHCl3, reflux, 2,5 h; 2.) CHCl3, reflux, 45 min
3: conc. HCl / 9 h / Heating
With
hydrogenchloride; toluene-4-sulfonic acid;
In
benzene;
DOI:10.1021/ja00311a046
- Guidance literature:
-
Multi-step reaction with 3 steps
1: p-toluenesulfonic acid / benzene / 2 h / Heating
2: 2.) 10percent aq. HCl / 1.) CHCl3, reflux, 2,5 h; 2.) CHCl3, reflux, 45 min
3: conc. HCl / 9 h / Heating
With
hydrogenchloride; toluene-4-sulfonic acid;
In
benzene;
DOI:10.1021/ja00311a046
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 72 percent / 6N aq. HCl/glacial acetic acid / 12 h / Heating
2: p-toluenesulfonic acid / benzene / 2 h / Heating
3: 2.) 10percent aq. HCl / 1.) CHCl3, reflux, 2,5 h; 2.) CHCl3, reflux, 45 min
4: conc. HCl / 9 h / Heating
With
hydrogenchloride; toluene-4-sulfonic acid; acetic acid;
In
benzene;
DOI:10.1021/ja00311a046
