(+)-(1S)-2-carbomethoxyadamantane-4-one 8-ethylene dithioketal

Base Information

• Chemical Name: (+)-(1S)-2-carbomethoxyadamantane-4-one 8-ethylene dithioketal
• CAS No.: 19087-16-2
• Molecular Formula: C₁₆H₂₂O₂S₄
• Molecular Weight: 374.613
• Mol file: 19087-16-2.mol

Synonyms:

Chemical Property of (+)-(1S)-2-carbomethoxyadamantane-4-one 8-ethylene dithioketal

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of (+)-(1S)-2-carbomethoxyadamantane-4-one 8-ethylene dithioketal

There total 1 articles about (+)-(1S)-2-carbomethoxyadamantane-4-one 8-ethylene dithioketal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

diazomethane (186581-53-3,908094-01-9,334-88-3) + ethane-1,2-dithiol (540-63-6) + (-)-(1S)-2-carboxyadamantane-4,8-dione (5202-69-7,19305-73-8,19305-74-9,98574-58-4) → (+)-(1S)-2-carbomethoxyadamantane-4-one 8-ethylene dithioketal (19305-78-3) + (+)-(1S)-2-carbomethoxyadamantane-4-one 8-ethylene dithioketal (19087-16-2)

Guidance literature:

With boron trifluoride diethyl etherate; Yield given. Multistep reaction. Yields of byproduct given; 1.) acetic acid, rt., 20 h; 2.) CH₂Cl₂/ether,;

DOI:10.1021/ja00311a046

upstream raw materials:

diazomethane

ethane-1,2-dithiol

(-)-(1S)-2-carboxyadamantane-4,8-dione