Technology Process of 2-METHYL-1-PENTADECENE
There total 7 articles about 2-METHYL-1-PENTADECENE which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
Pd(P(t-Bu)2Me)2; potassium tert-butylate; N-cyclohexyl-cyclohexanamine;
In
1,4-dioxane;
at 20 ℃;
for 24h;
Concentration;
Kinetics;
Inert atmosphere;
DOI:10.1021/ja306323x
- Guidance literature:
-
With
Pd(P(t-Bu)2Me)2; potassium tert-butylate; N-cyclohexyl-cyclohexanamine;
In
1,4-dioxane;
at 80 ℃;
for 8h;
Inert atmosphere;
DOI:10.1021/ja306323x
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: sodium hydride / tetrahydrofuran / 0 °C / Inert atmosphere
1.2: 20 °C / Inert atmosphere
2.1: 10% Pd/C; hydrogen / methanol / 18 h / 20 °C / 760.05 Torr
3.1: lithium aluminium tetrahydride / diethyl ether / 0 - 20 h
4.1: dmap; triethylamine / dichloromethane / 0 - 20 °C / Inert atmosphere
5.1: Pd(P(t-Bu)2Me)2; potassium tert-butylate; N-cyclohexyl-cyclohexanamine / 1,4-dioxane / 8 h / 80 °C / Inert atmosphere
With
dmap; lithium aluminium tetrahydride; Pd(P(t-Bu)2Me)2; 10% Pd/C; potassium tert-butylate; hydrogen; sodium hydride; triethylamine; N-cyclohexyl-cyclohexanamine;
In
tetrahydrofuran; 1,4-dioxane; methanol; diethyl ether; dichloromethane;
DOI:10.1021/ja306323x
