3,6-dibromo-9-(4-biphenylyl)carbazole

Base Information

Chemical Name:3,6-dibromo-9-(4-biphenylyl)carbazole
CAS No.:894791-50-5
Molecular Formula:C24H15Br2N
Molecular Weight:477.198
Hs Code.:
Mol file:894791-50-5.mol

Synonyms:3,6-dibromo-9-(4-biphenylyl)carbazole;9-([1,1'-biphenyl]-4-yl)-3,6-dibromo-9H-carbazole

Suppliers and Price of 3,6-dibromo-9-(4-biphenylyl)carbazole

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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Total 14 raw suppliers

Chemical Property of 3,6-dibromo-9-(4-biphenylyl)carbazole

Chemical Property:

Melting Point:218 - 219 °C
PSA：4.93000
LogP:7.97570

Purity/Quality:: 98% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

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Technology Process of 3,6-dibromo-9-(4-biphenylyl)carbazole

There total 5 articles about 3,6-dibromo-9-(4-biphenylyl)carbazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 6299-16-7
9-([1,1’-biphenyl]-4-yl)-9H-carbazole

: 894791-50-5
9-([1,1'-biphenyl]-4-yl)-3,6-dibromo-9H-carbazole

Guidance literature:: With N-Bromosuccinimide; In acetic acid; ethyl acetate; toluene; for 100h;

Reference yield:

: 255829-38-0
3,6-dibromo-9-(4-iodo-phenyl)-9H-carbazole

: 98-80-6
phenylboronic acid

: 894791-50-5
9-([1,1'-biphenyl]-4-yl)-3,6-dibromo-9H-carbazole

Guidance literature:: With triphenylphosphine; palladium dichloride; In N,N-dimethyl acetamide; at 120 ℃; for 6h; Temperature;
DOI:10.1039/c5ra26698j

Reference yield:

: 352-34-1
4-fluoro-1-iodobenzene

: 894791-50-5
9-([1,1'-biphenyl]-4-yl)-3,6-dibromo-9H-carbazole

Guidance literature:: Multi-step reaction with 2 steps

1: caesium carbonate / N,N-dimethyl acetamide / 24 h / 150 °C

2: triphenylphosphine; palladium dichloride / N,N-dimethyl acetamide / 6 h / 120 °C

With caesium carbonate; triphenylphosphine; palladium dichloride; In N,N-dimethyl acetamide; 2: |Suzuki Coupling;
DOI:10.1039/c5ra26698j