8-METHOXY-1-METHYL-2,3,4,5-TETRAHYDRO-1H-3-BENZAZEPINE

Base Information

Chemical Name:8-METHOXY-1-METHYL-2,3,4,5-TETRAHYDRO-1H-3-BENZAZEPINE
CAS No.:849663-07-6
Molecular Formula:C12H17NO
Molecular Weight:191.273
Hs Code.:
Mol file:849663-07-6.mol

Synonyms:8-METHOXY-1-METHYL-2,3,4,5-TETRAHYDRO-1H-3-BENZAZEPINE

Suppliers and Price of 8-METHOXY-1-METHYL-2,3,4,5-TETRAHYDRO-1H-3-BENZAZEPINE

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
8-METHOXY-1-METHYL-2,3,4,5-TETRAHYDRO-1H-3-BENZAZEPINE 95.00%
5MG
$ 504.96

Total 2 raw suppliers

Chemical Property of 8-METHOXY-1-METHYL-2,3,4,5-TETRAHYDRO-1H-3-BENZAZEPINE

Chemical Property:

PSA：21.26000
LogP:2.27320

Purity/Quality:

97% ^*data from raw suppliers

8-METHOXY-1-METHYL-2,3,4,5-TETRAHYDRO-1H-3-BENZAZEPINE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 8-METHOXY-1-METHYL-2,3,4,5-TETRAHYDRO-1H-3-BENZAZEPINE

There total 4 articles about 8-METHOXY-1-METHYL-2,3,4,5-TETRAHYDRO-1H-3-BENZAZEPINE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 849663-11-2
8-methoxy-1-methyl-1,3,4,5-tetrahydro-benzo[d]azepin-2-one

: 849663-07-6
8-methoxy-1-methyl-2,3,4,5-tetrahydro-1H-benzo[d]azepine

Guidance literature:: 8-methoxy-1-methyl-1,3,4,5-tetrahydro-benzo[d]azepin-2-one; With borane-THF; In tetrahydrofuran; at 0 ℃; for 4h; Heating / reflux;

With hydrogenchloride; In water; at 100 ℃; for 1h;

With sodium hydroxide; In water;

Reference yield:

: 1465246-40-5
C₁₂H₁₈ClNO

: 849663-07-6
8-methoxy-1-methyl-2,3,4,5-tetrahydro-1H-benzo[d]azepine

Guidance literature:: With aluminium trichloride; at 140 ℃; for 4h;
DOI:10.1021/jm0709034

Reference yield:

: 34162-29-3
2-chloro-N-[2-(4-methoxyphenyl)ethyl]propionamide

: 849663-07-6
8-methoxy-1-methyl-2,3,4,5-tetrahydro-1H-benzo[d]azepine

Guidance literature:: Multi-step reaction with 2 steps

1: AlCl₃ / 150 - 200 °C

2: BH₃ / diethyl ether

With aluminium trichloride; borane; In diethyl ether; 1: Friedel-Crafts cyclization;
DOI:10.1016/j.bmcl.2004.12.080