8-methoxy-1-methyl-3-[5-(4-trifluoromethyl-phenyl)-furan-2-ylmethyl]-2,3,4,5-tetrahydro-1H-benzo[d]azepine

Base Information

Chemical Name:8-methoxy-1-methyl-3-[5-(4-trifluoromethyl-phenyl)-furan-2-ylmethyl]-2,3,4,5-tetrahydro-1H-benzo[d]azepine
CAS No.:952710-37-1
Molecular Formula:C₂₄H₂₄F₃NO₂
Molecular Weight:415.455
Hs Code.:

Synonyms:8-methoxy-1-methyl-3-[5-(4-trifluoromethyl-phenyl)-furan-2-ylmethyl]-2,3,4,5-tetrahydro-1H-benzo[d]azepine

Suppliers and Price of 8-methoxy-1-methyl-3-[5-(4-trifluoromethyl-phenyl)-furan-2-ylmethyl]-2,3,4,5-tetrahydro-1H-benzo[d]azepine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 8-methoxy-1-methyl-3-[5-(4-trifluoromethyl-phenyl)-furan-2-ylmethyl]-2,3,4,5-tetrahydro-1H-benzo[d]azepine

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 8-methoxy-1-methyl-3-[5-(4-trifluoromethyl-phenyl)-furan-2-ylmethyl]-2,3,4,5-tetrahydro-1H-benzo[d]azepine

There total 1 articles about 8-methoxy-1-methyl-3-[5-(4-trifluoromethyl-phenyl)-furan-2-ylmethyl]-2,3,4,5-tetrahydro-1H-benzo[d]azepine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 55377-77-0
5-(4-(trifluoromethyl)phenyl)furan-2-carbaldehyde

: 849663-07-6
8-methoxy-1-methyl-2,3,4,5-tetrahydro-1H-benzo[d]azepine

: 952710-37-1
8-methoxy-1-methyl-3-[5-(4-trifluoromethyl-phenyl)-furan-2-ylmethyl]-2,3,4,5-tetrahydro-1H-benzo[d]azepine

Guidance literature:: 5-(4-(trifluoromethyl)phenyl)furan-2-carbaldehyde; 8-methoxy-1-methyl-2,3,4,5-tetrahydro-1H-benzo[d]azepine; With acetic acid; In 1,1-dichloroethane; at 20 ℃; for 16h;

With sodium tris(acetoxy)borohydride; In 1,1-dichloroethane; at 20 ℃; for 24h;

With sodium hydroxide; In 1,1-dichloroethane; water;

Reference yield: 100.0%

: 952710-37-1
8-methoxy-1-methyl-3-[5-(4-trifluoromethyl-phenyl)-furan-2-ylmethyl]-2,3,4,5-tetrahydro-1H-benzo[d]azepine

: 952710-38-2
5-methyl-3-[5-(4-trifluoromethyl-phenyl)-furan-2-ylmethyl]-2,3,4,5-tetrahydro-1H-benzo[d]azepin-7-ol

Guidance literature:: 8-methoxy-1-methyl-3-[5-(4-trifluoromethyl-phenyl)-furan-2-ylmethyl]-2,3,4,5-tetrahydro-1H-benzo[d]azepine; With water; hydrogen bromide; acetic acid; at 80 ℃; for 17h;

With potassium carbonate; In water; ethyl acetate; pH=9;