ethyl 6-phenylH-imidazo[1,2-a]pyridine-2-carboxylate

Base Information

• Chemical Name: ethyl 6-phenylH-imidazo[1,2-a]pyridine-2-carboxylate
• CAS No.: 1173694-01-3
• Molecular Formula: C16H14N2O2
• Molecular Weight: 266.299
• Hs Code.: 2933990090
• Mol file: 1173694-01-3.mol

Synonyms:ethyl 6-phenylH-imidazo[1,2-a]pyridine-2-carboxylate;Ethyl 6-phenyimidazo[1,2-a]pyridine-2-carboxylate

Chemical Property of ethyl 6-phenylH-imidazo[1,2-a]pyridine-2-carboxylate

Chemical Property:

• PSA: 43.60000
• LogP: 3.17800
• Storage Temp.: 2-8°C

Purity/Quality:

97% ^*data from raw suppliers

Ethyl6-phenylimidazo[1,2-a]pyridine-2-carboxylate ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of ethyl 6-phenylH-imidazo[1,2-a]pyridine-2-carboxylate

There total 3 articles about ethyl 6-phenylH-imidazo[1,2-a]pyridine-2-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

ethyl 6-bromoimidazo<1,2-a>pyridine-2-carboxylate (67625-37-0) + phenylboronic acid (98-80-6) → 6-phenylimidazo[1,2-a]pyridine-2-carboxylic acid ethyl ester (1173694-01-3)

Guidance literature:

With potassium fluoride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In water; acetonitrile; at 160 ℃; for 0.0833333h; Microwaves;

Reference yield:

ethyl 6-iodo-1H-imidazo[1,2-a]pyridine-2-carboxylate (214958-32-4) + phenylboronic acid (98-80-6) → 6-phenylimidazo[1,2-a]pyridine-2-carboxylic acid ethyl ester (1173694-01-3)

Guidance literature:

With bis(di-tert-?butyl(4-?dimethylaminophenyl)?phosphine)?dichloropalladium(II); caesium carbonate; In 1,4-dioxane; water;

Reference yield:

→ 6-phenylimidazo[1,2-a]pyridine-2-carboxylic acid ethyl ester (1173694-01-3)

Guidance literature:

With dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; sodium carbonate; In 1,2-dimethoxyethane; water; at 80 ℃; for 16h; Inert atmosphere;

upstream raw materials:

ethyl 6-bromoimidazo<1,2-a>pyridine-2-carboxylate

phenylboronic acid

ethyl 6-iodo-1H-imidazo[1,2-a]pyridine-2-carboxylate

Downstream raw materials:

6-phenylimidazo[1,2-a]pyridine-2-carboxylic acid

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