(1R,2S,3R,4S)-3-(tert-butoxycarbonylamino)bicyclo[2.2.1]hept-5-ene-2-carboxylic acid

Base Information

• Chemical Name: (1R,2S,3R,4S)-3-(tert-butoxycarbonylamino)bicyclo[2.2.1]hept-5-ene-2-carboxylic acid
• CAS No.: 1242184-48-0
• Molecular Formula: C13H19NO4
• Molecular Weight: 253.29426
• Hs Code.: 2924297099
• Mol file: 1242184-48-0.mol

Synonyms:(1R,2S,3R,4S)-3-(tert-butoxycarbonylamino)bicyclo[2.2.1]hept-5-ene-2-carboxylic acid

Chemical Property of (1R,2S,3R,4S)-3-(tert-butoxycarbonylamino)bicyclo[2.2.1]hept-5-ene-2-carboxylic acid

Chemical Property:

Purity/Quality:

98% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (1R,2S,3R,4S)-3-(tert-butoxycarbonylamino)bicyclo[2.2.1]hept-5-ene-2-carboxylic acid

There total 37 articles about (1R,2S,3R,4S)-3-(tert-butoxycarbonylamino)bicyclo[2.2.1]hept-5-ene-2-carboxylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

3-endo-N-tert-butyloxycarbonylaminobicyclo<2.2.1>hept-5-ene-2-endo carboxylate de methyle → (1SR,2RS,3SR,4RS)-3-tert-butoxycarbonylaminobicyclo[2.2.1]hept-5-ene-2-carboxylic acid (1242184-48-0,1242184-46-8,148257-06-1)

Guidance literature:

With sodium hydroxide; In methanol; for 2h; Ambient temperature;

DOI:10.1016/S0040-4020(01)86298-0

Reference yield: 98.0%

3-exo-N-tert-butyloxycarbonylaminobicyclo<2.2.1>hept-5-ene-2-exo carboxylate de methyle → Acide-3-exo-N-tert-butyloxycarbonylaminobicyclo<2.2.1>hept-5-ene-2-exo carboxylique (1242184-48-0,1242184-46-8,148257-06-1)

Guidance literature:

With sodium hydroxide; In methanol; for 2h; Ambient temperature;

DOI:10.1016/S0040-4020(01)86298-0

Reference yield: 95.0%

(2S,3R)-3-exo-(tert-Butyloxycarbonylamino)-bicyclo[2.2.1]hept-5-ene-2-exo-carboxylic acid methyl ester → (1S,2S,3R,4R)-3-exo-N-tbutyloxycarbonylaminobicyclo[2,2,1]hept-5-ene-2-exo-carboxylic acid (887908-99-8,1242184-48-0,1242184-46-8,148257-06-1)

Guidance literature:

With water; lithium hydroxide; In tetrahydrofuran; for 1h;

DOI:10.1002/chem.200902332

upstream raw materials:

di-tert-butyl dicarbonate

(1SR,2RS,3SR,4RS)-3-aminobicyclo[2.2.1]hept-5-ene-2-carboxylic acid

3-exo-aminobicyclo[2.2.1]hept-5-ene-2-exo-carboxylic acid

(1SR,2SR,5RS,6RS)-4-oxo-3-aza-tricyclo[4.2.1.0(2,5)]non-7-ene-3-carboxylic acid tert-butyl ester

Downstream raw materials:

(1S,2S,3R,4R)-3-exo-N-^tbutyloxycarbonylaminobicyclo[2,2,1]hept-5-ene-2-exo-carboxylic acid

(1R,2R,3S,4S)-3-exo-N-^tbutyloxycarbonylaminobicyclo[2,2,1]hept-5-ene-2-exo-carboxylic acid

CEP-28122

(1S,2S,3R,4R)-3-(6-chloro-2-(4-morpholinophenyl)-3H-imidazo[4,5-b]pyridin-7-ylamino)-N-methylbicyclo[2.2.1]hept-5-ene-2-carboxamide

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