3-ENDO-AMINOBICYCLO[2.2.1]HEPT-5-ENE-2-ENDO-CARBOXYLIC ACID

Base Information

• Chemical Name: 3-ENDO-AMINOBICYCLO[2.2.1]HEPT-5-ENE-2-ENDO-CARBOXYLIC ACID
• CAS No.: 88330-29-4
• Molecular Formula: C₈H₁₁NO₂
• Molecular Weight: 153.181
• Hs Code.: 29224985
• Mol file: 88330-29-4.mol

Synonyms:Bicyclo[2.2.1]hept-5-ene-2-carboxylicacid, 3-amino-, (endo,endo)-; diendo-(1RS,2RS,3SR,4SR)-3-Amino-5-bicyclo[2.2.1]heptene-2-carboxylicacid; endo,endo-3-Amino-5-bicyclo[2.2.1]heptene-2-carboxylic acid

Chemical Property of 3-ENDO-AMINOBICYCLO[2.2.1]HEPT-5-ENE-2-ENDO-CARBOXYLIC ACID

Chemical Property:

• Vapor Pressure: 0mmHg at 25°C
• Melting Point: 265-267 °C
• Refractive Index: 1.4640 (estimate)
• Boiling Point: 309.156°C at 760 mmHg
• Flash Point: 140.773°C
• PSA: 63.32000
• Density: 1.294
• LogP: 0.92070

Purity/Quality:

98%min ^*data from raw suppliers

3-Aminobicyclo[2.2.1]hept-5-ene-2-carboxylic acid hydrochloride ^*data from reagent suppliers

Safty Information:

• Safety Statements: 24/25

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 3-ENDO-AMINOBICYCLO[2.2.1]HEPT-5-ENE-2-ENDO-CARBOXYLIC ACID

There total 3 articles about 3-ENDO-AMINOBICYCLO[2.2.1]HEPT-5-ENE-2-ENDO-CARBOXYLIC ACID which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3,6-endomethylene-1,2,3,6-tetrahydrophthalic anhydride (129-64-6) → (1SR,2RS,3SR,4RS)-3-aminobicyclo[2.2.1]hept-5-ene-2-carboxylic acid (88330-29-4,202187-27-7,202187-24-4,202187-28-8,202187-29-9)

Guidance literature:

With ammonium hydroxide; sodium hydroxide; sodium hypochlorite; Yield given. Multistep reaction; 1.) 0 deg C; 2.) 70 deg C, 5 min.;

DOI:10.1002/jhet.5570200509

Reference yield:

cis-N-sulphonyloxy-5-norbornene-endo-2,3-dicarboximide (5433-80-7) → (1SR,2RS,3SR,4RS)-3-aminobicyclo[2.2.1]hept-5-ene-2-carboxylic acid (88330-29-4,202187-27-7,202187-24-4,202187-28-8,202187-29-9)

Guidance literature:

With sodium hydroxide;

DOI:10.1021/jo01091a035

Reference yield:

endo-N-hydroxy-5-norbornene-2,3-dicarboxyimide (21715-90-2,397299-61-5) → (1SR,2RS,3SR,4RS)-3-aminobicyclo[2.2.1]hept-5-ene-2-carboxylic acid (88330-29-4,202187-27-7,202187-24-4,202187-28-8,202187-29-9)

Guidance literature:

Multi-step reaction with 2 steps

1: chloroform; triethylamine

2: aqueous NaOH

With sodium hydroxide; chloroform; triethylamine;

DOI:10.1021/jo01091a035

upstream raw materials:

cis-N-sulphonyloxy-5-norbornene-endo-2,3-dicarboximide

3,6-endomethylene-1,2,3,6-tetrahydrophthalic anhydride

endo-N-hydroxy-5-norbornene-2,3-dicarboxyimide

Downstream raw materials:

(1S,2R,3S,4R)-3-(4-Chloro-benzoylamino)-bicyclo[2.2.1]hept-5-ene-2-carboxylic acid

(1S,2R,3S,4R)-3-[3-(4-Chloro-phenyl)-thioureido]-bicyclo[2.2.1]hept-5-ene-2-carboxylic acid

(1R,2S,3R,4S)-3-(3,4-Dichloro-benzoylamino)-bicyclo[2.2.1]hept-5-ene-2-carboxylic acid

3-phenyl-2-thioxo-2,3,r-4a,t-5,t-8,c-8a-hexahydro-5,8-methanoquinazolin-4(1H)-one

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