1-(Phenylsulphonyl)-2-iodo-4-nitro-7-azaindole

Base Information

Chemical Name:1-(Phenylsulphonyl)-2-iodo-4-nitro-7-azaindole
CAS No.:1227268-92-9
Molecular Formula:C13H8IN3O4S
Molecular Weight:429.18979
Hs Code.:
Mol file:1227268-92-9.mol

Synonyms:1-(Phenylsulphonyl)-2-iodo-4-nitro-7-azaindole;1-(phenylsulfonyl)-2-iodo-4-nitro-7-azaindole

Suppliers and Price of 1-(Phenylsulphonyl)-2-iodo-4-nitro-7-azaindole

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 2 raw suppliers

Chemical Property of 1-(Phenylsulphonyl)-2-iodo-4-nitro-7-azaindole

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 1-(Phenylsulphonyl)-2-iodo-4-nitro-7-azaindole

There total 2 articles about 1-(Phenylsulphonyl)-2-iodo-4-nitro-7-azaindole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1-(benzenesulfonyl)-4-nitro-1H-pyrrolo[2,3-b]pyridine

: 1227268-92-9
1-(benzenesulfonyl)-2-iodo-4-nitro-1H-pyrrolo[2,3-b]pyridine

Guidance literature:: 1-(benzenesulfonyl)-4-nitro-1H-pyrrolo[2,3-b]pyridine; With 2,2,6,6-tetramethylpiperidinyl-lithium; In tetrahydrofuran; at -78 ℃; for 1h;

With iodine; In tetrahydrofuran; at -78 ℃; for 1h;

Reference yield:

: 83683-82-3
4-nitro-1H-pyrrolo<2,3-b>pyridine

: 98-09-9
benzenesulfonyl chloride

: 1227268-92-9
1-(benzenesulfonyl)-2-iodo-4-nitro-1H-pyrrolo[2,3-b]pyridine

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydride / mineral oil; tetrahydrofuran / 1 h / 0 °C

1.2: 1 h / 0 °C

2.1: 2,2,6,6-tetramethylpiperidinyl-lithium / tetrahydrofuran / 1 h / -78 °C

2.2: 1 h / -78 °C

With 2,2,6,6-tetramethylpiperidinyl-lithium; sodium hydride; In tetrahydrofuran; mineral oil;