5-iodo-1,3-benzenedimethanol

Base Information

Chemical Name:5-iodo-1,3-benzenedimethanol
CAS No.:859238-49-6
Molecular Formula:C8H9IO2
Molecular Weight:264.063
Hs Code.:
Mol file:859238-49-6.mol

Synonyms:5-iodo-1,3-benzenedimethanol;(3-Hydroxymethyl-5-iodo-phenyl)-methanol

Suppliers and Price of 5-iodo-1,3-benzenedimethanol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Chemcia Scientific
(3-Hydroxymethyl-5-iodo-phenyl)-methanol 95%
5 G
$ 555.00

AK Scientific
[3-(Hydroxymethyl)-5-iodophenyl]methanol
5g
$ 822.00

AK Scientific
[3-(Hydroxymethyl)-5-iodophenyl]methanol
1g
$ 349.00

Total 1 raw suppliers

Chemical Property of 5-iodo-1,3-benzenedimethanol

Chemical Property:

PSA：40.46000
LogP:1.27580

Purity/Quality:: (3-Hydroxymethyl-5-iodo-phenyl)-methanol 95% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 5-iodo-1,3-benzenedimethanol

There total 5 articles about 5-iodo-1,3-benzenedimethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 51839-15-7
5-iodo-isophthalic acid dimethyl ester

: 859238-49-6
(3-hydroxymethyl-5-iodo-phenyl)-methanol

Guidance literature:: With diisobutylaluminium hydride; In dichloromethane; for 6h; Heating;
DOI:10.1080/00397910601033435

Reference yield: 74.0%

: 51839-15-7
5-iodo-isophthalic acid dimethyl ester

: 177734-81-5
5-Hydroxymethyl-3-iodobenzoic acid methyl ester

: 859238-49-6
(3-hydroxymethyl-5-iodo-phenyl)-methanol

Guidance literature:: With sodium tetrahydroborate; In tetrahydrofuran; at 50 ℃; for 2h; Inert atmosphere;
DOI:10.1021/acsmedchemlett.1c00156

Reference yield:

: 51839-16-8
5-iodoisophthalic acid

: 859238-49-6
(3-hydroxymethyl-5-iodo-phenyl)-methanol

Guidance literature:: Multi-step reaction with 2 steps

1: 96 percent / H₂SO₄

2: 79 percent / LiAlH₄ / diethyl ether

With lithium aluminium tetrahydride; sulfuric acid; In diethyl ether;
DOI:10.1021/ja960317s