1,4-Anhydro-5-O,6-O-isopropylidene-D-glucitol bis(methanesulfonate)

Base Information

Chemical Name:1,4-Anhydro-5-O,6-O-isopropylidene-D-glucitol bis(methanesulfonate)
CAS No.:55730-75-1
Molecular Formula:C11H20O9S2
Molecular Weight:360.4
Hs Code.:
Mol file:55730-75-1.mol

Synonyms:1,4-Anhydro-5-O,6-O-isopropylidene-D-glucitol bis(methanesulfonate)

Suppliers and Price of 1,4-Anhydro-5-O,6-O-isopropylidene-D-glucitol bis(methanesulfonate)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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Total 1 raw suppliers

Chemical Property of 1,4-Anhydro-5-O,6-O-isopropylidene-D-glucitol bis(methanesulfonate)

Chemical Property:

Melting Point:163 - 163.5 °C (ethanol)
PSA：131.19000
LogP:1.38790

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 1,4-Anhydro-5-O,6-O-isopropylidene-D-glucitol bis(methanesulfonate)

There total 2 articles about 1,4-Anhydro-5-O,6-O-isopropylidene-D-glucitol bis(methanesulfonate) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 124-63-0
methanesulfonyl chloride

: 55730-73-9,86362-57-4
(2S,3R,4S)-2-(2,2-Dimethyl-[1,3]dioxolan-4-yl)-tetrahydro-furan-3,4-diol

: 55730-74-0
1,4-anhydro-5,6-O-isopropylidene-2-O-methanesulfonyl-D-glucitol

: 55730-75-1
Methanesulfonic acid (2R,3S,4S)-2-(2,2-dimethyl-[1,3]dioxolan-4-yl)-4-methanesulfonyloxy-tetrahydro-furan-3-yl ester

Guidance literature:: With pyridine; at 0 ℃; for 24h; Yield given. Yields of byproduct given;
DOI:10.1016/S0008-6215(00)90454-3

Reference yield:

: 7726-97-8,10334-28-8,20662-31-1,22554-76-3,22554-77-4,22554-79-6,27299-12-3,28218-56-6,32742-35-1,40026-08-2,51196-40-8,51607-77-3,53648-56-9,96243-58-2,124379-08-4,124379-13-1
1,4-anhydro-D-glucitol

: 55730-75-1
Methanesulfonic acid (2R,3S,4S)-2-(2,2-dimethyl-[1,3]dioxolan-4-yl)-4-methanesulfonyloxy-tetrahydro-furan-3-yl ester

Guidance literature:: Multi-step reaction with 2 steps

1: acetyl chloride, ethanol / dimethylformamide / 6 h / Ambient temperature

2: pyridine / 24 h / 0 °C

With pyridine; ethanol; acetyl chloride; In N,N-dimethyl-formamide;
DOI:10.1016/S0008-6215(00)90454-3