4-(4-bromophenyl)tetrahydro-2H-Pyran-4-carboxylic acid ethyl ester

Base Information

Chemical Name:4-(4-bromophenyl)tetrahydro-2H-Pyran-4-carboxylic acid ethyl ester
CAS No.:1227160-22-6
Molecular Formula:C₁₄H₁₇BrO₃
Molecular Weight:313.191
Hs Code.:

Synonyms:4-(4-bromophenyl)tetrahydro-2H-Pyran-4-carboxylic acid ethyl ester;ethyl 4-(4-bromophenyl)tetrahydro-2H-pyran-4-carboxylate

Suppliers and Price of 4-(4-bromophenyl)tetrahydro-2H-Pyran-4-carboxylic acid ethyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 2 raw suppliers

Chemical Property of 4-(4-bromophenyl)tetrahydro-2H-Pyran-4-carboxylic acid ethyl ester

Chemical Property:

Purity/Quality:: more than 98% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 4-(4-bromophenyl)tetrahydro-2H-Pyran-4-carboxylic acid ethyl ester

There total 2 articles about 4-(4-bromophenyl)tetrahydro-2H-Pyran-4-carboxylic acid ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

: 5414-19-7
1,1'-oxybis(2-bromo-ethane)

: 14062-25-0
Ethyl 4-bromophenylacetate

: 1227160-22-6
ethyl 4-(4-bromophenyl)tetrahydro-2H-pyran-4-carboxylate

Guidance literature:: With sodium hydride; In diethyl ether; N,N-dimethyl-formamide; mineral oil; at 0 - 20 ℃; for 17h;

Reference yield: 17.0%

: 14062-25-0
Ethyl 4-bromophenylacetate

: 111-44-4
3-oxa-1,5-dichloropentane

: 1227160-22-6
ethyl 4-(4-bromophenyl)tetrahydro-2H-pyran-4-carboxylate

Guidance literature:: Ethyl 4-bromophenylacetate; With sodium hydride; In N,N-dimethyl-formamide; mineral oil; for 0.166667h;

With 15-crown-5; In N,N-dimethyl-formamide; mineral oil; at 20 ℃; for 0.5h;

3-oxa-1,5-dichloropentane; With sodium iodide; In N,N-dimethyl-formamide; mineral oil; at 20 ℃; for 12h;

Reference yield: 99.0%

: 1227160-22-6
ethyl 4-(4-bromophenyl)tetrahydro-2H-pyran-4-carboxylate

: 1152567-60-6
1-(4-bromophenyl)tetrahydro-2H-pyran-4-carboxylic acid

Guidance literature:: ethyl 4-(4-bromophenyl)tetrahydro-2H-pyran-4-carboxylate; With sodium hydroxide; In 1,4-dioxane; for 42h; Reflux;

With hydrogenchloride; In 1,4-dioxane; water; at 20 ℃; for 0.25h;