14-doxylstearic acid

Base Information

• Chemical Name: 14-doxylstearic acid
• CAS No.: 61443-70-7
• Molecular Formula: C22H42NO4*
• Molecular Weight: 384.57318
• Mol file: 61443-70-7.mol

Synonyms:14-doxylstearic acid

Chemical Property of 14-doxylstearic acid

Chemical Property:

Purity/Quality:

14-Doxylstearic Acid ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 14-doxylstearic acid

There total 2 articles about 14-doxylstearic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N-(2-hydroxy-1,1-dimethylethyl)-13-(2-butyl-3-ylooxy-4,4-dimethyl-1,3-oxazolidin-2-yl)tridecanamide → 2-butyl-2-(12-carboxy-dodecyl)-4,4-dimethyl-oxazolidin-3-yloxyl (50614-00-1,61443-70-7)

Guidance literature:

With sodium hydroxide; In 1,4-dioxane; at 60 ℃; for 24h;

DOI:10.1081/SCC-200032488

Reference yield:

methyl-14-oxooctadecanoate (2380-29-2) → 2-butyl-2-(12-carboxy-dodecyl)-4,4-dimethyl-oxazolidin-3-yloxyl (50614-00-1,61443-70-7)

Guidance literature:

Multi-step reaction with 2 steps

1.1: p-toluenesulfonic acid monohydrate / toluene / 216 h / Heating

1.2: 24.2 percent / 3-chloroperoxybenzoic acid / diethyl ether / 14 h / cooling

2.1: NaOH / dioxane / 24 h / 60 °C

With sodium hydroxide; toluene-4-sulfonic acid; In 1,4-dioxane; toluene;

DOI:10.1081/SCC-200032488

upstream raw materials:

methyl-14-oxooctadecanoate

Refernces