Synthetic Communications p. 3763 - 3771 (2004)
Update date:2022-08-03
Topics:
Mravljak, Janez
Pecar, Slavko
Paramagnetic amide side products (6a-g) have been isolated from the reaction mixture in the synthesis of spin-labeled fatty acids of the doxyl type. After their hydrolysis to the corresponding acid, 7, the overall yield of spin-labeled fatty acids is significantly increased compared with published procedures.
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