[4-(2-AMINO-ETHYL)-PHENYL]-METHANOL HYDROCHLORIDE

Base Information

• Chemical Name: [4-(2-AMINO-ETHYL)-PHENYL]-METHANOL HYDROCHLORIDE
• CAS No.: 68559-71-7
• Molecular Formula: C9H14ClNO
• Molecular Weight: 0
• Hs Code.: 2922199090
• Mol file: 68559-71-7.mol

Synonyms:[4-(2-AMINO-ETHYL)-PHENYL]-METHANOL HYDROCHLORIDE

Chemical Property of [4-(2-AMINO-ETHYL)-PHENYL]-METHANOL HYDROCHLORIDE

Chemical Property:

• PSA: 46.25000
• LogP: 2.18240

Purity/Quality:

97% ^*data from raw suppliers

[4-(2-Aminoethyl)phenyl]methanolHydrochloride ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of [4-(2-AMINO-ETHYL)-PHENYL]-METHANOL HYDROCHLORIDE

There total 6 articles about [4-(2-AMINO-ETHYL)-PHENYL]-METHANOL HYDROCHLORIDE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-(2-aminoethyl)-benzyl alcohol (64353-30-6) → [4-(2-Amino-ethyl)-phenyl]-methanol hydrochloride (68559-71-7)

Guidance literature:

With hydrogenchloride; In diethyl ether; isopropyl alcohol; at 0 ℃; for 0.166667h;

DOI:10.1039/c6cc04954k

Reference yield:

(4-(2-nitrovinyl)phenyl)methanol → [4-(2-Amino-ethyl)-phenyl]-methanol hydrochloride (68559-71-7)

Guidance literature:

Multi-step reaction with 3 steps

1: sodium tetrahydroborate; acetic acid / dimethyl sulfoxide / 0.5 h / 0 - 20 °C

2: palladium 10% on activated carbon; hydrogen / methanol / 8 h

3: hydrogenchloride / isopropyl alcohol; diethyl ether / 0.17 h / 0 °C

With hydrogenchloride; sodium tetrahydroborate; palladium 10% on activated carbon; hydrogen; acetic acid; In methanol; diethyl ether; dimethyl sulfoxide; isopropyl alcohol;

DOI:10.1039/c6cc04954k

Reference yield:

(4-(2-nitroethyl)phenyl)methanol → [4-(2-Amino-ethyl)-phenyl]-methanol hydrochloride (68559-71-7)

Guidance literature:

Multi-step reaction with 2 steps

1: palladium 10% on activated carbon; hydrogen / methanol / 8 h

2: hydrogenchloride / isopropyl alcohol; diethyl ether / 0.17 h / 0 °C

With hydrogenchloride; palladium 10% on activated carbon; hydrogen; In methanol; diethyl ether; isopropyl alcohol;

DOI:10.1039/c6cc04954k

upstream raw materials:

terephthalaldehyde,

4-(hydroxylmethyl)benzaldehyde

4-(2-aminoethyl)-benzyl alcohol

Downstream raw materials:

2-(9H-Fluoren-9-yl)-N-[2-(4-hydroxymethyl-phenyl)-ethyl]-acetamide

tert-butyl N-{2-[4-(hydroxymethyl)phenyl]ethyl}carbamate

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