5,8-Dimethylbenzo[c]phenanthrene

Base Information

Chemical Name:5,8-Dimethylbenzo[c]phenanthrene
CAS No.:54986-63-9
Molecular Formula:C₂₀H₁₆
Molecular Weight:256.347
Hs Code.:2902909090
European Community (EC) Number:662-947-1
DSSTox Substance ID:DTXSID60970336
Nikkaji Number:J103.325E
Wikidata:Q82953515
Mol file:54986-63-9.mol

Synonyms:5,8-Dimethylbenzo[c]phenanthrene;54986-63-9;Benzo[c]phenanthrene, 5,8-dimethyl-;Benzo(c)phenanthrene, 5,8-dimethyl-;DTXSID60970336;PKNNRYLZAYRCOT-UHFFFAOYSA-N;5,8-dimethylbenzo[c]-phenanthrene;5,8-Dimethylbenzo[c]phenanthrene #;AKOS024341219;AR-G51 5,8-DIMETHYLBENZO(C)PHENANTHRENE

Suppliers and Price of 5,8-Dimethylbenzo[c]phenanthrene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Sigma-Aldrich
AR-G51 5,8-DIMETHYLBENZO(C)PHENANTHRENE Aldrich
1ea
$ 57.00

Total 2 raw suppliers

Chemical Property of 5,8-Dimethylbenzo[c]phenanthrene

Chemical Property:

Vapor Pressure:2.75E-08mmHg at 25°C
Refractive Index:1.7290 (estimate)
Boiling Point:462.3°C at 760 mmHg
Flash Point:226.6°C
PSA：0.00000
Density:1.142g/cm³
LogP:5.76300
XLogP3:6.4
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:0
Rotatable Bond Count:0
Exact Mass:256.125200510
Heavy Atom Count:20
Complexity:314

Purity/Quality:

99% ^*data from raw suppliers

AR-G51 5,8-DIMETHYLBENZO(C)PHENANTHRENE Aldrich ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC1=CC2=C(C3=CC=CC=C13)C4=CC=CC=C4C(=C2)C

Technology Process of 5,8-Dimethylbenzo[c]phenanthrene

There total 8 articles about 5,8-Dimethylbenzo[c]phenanthrene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 1047647-76-6
5,6,7,8-tetrahydro-5,8-dimethylbenzo[c]phenanthrene

: 54986-63-9
5,8-dimethylbenzo[c]phenanthrene

Guidance literature:: With 10% Pd/C; In 1,3,5-trimethyl-benzene; for 9h; Reflux;
DOI:10.1002/anie.200801396

Reference yield:

: 93878-28-5
β-Benzhydrylglutaric acid

: 54986-63-9
5,8-dimethylbenzo[c]phenanthrene

Guidance literature:: Multi-step reaction with 2 steps

1: PCl₅ / Behandeln des Reaktionsprodukts mit AlCl₃ in Tetrachloraethan, zuletzt bei 60grad

2: diethyl ether; xylene / aufeinanderfolgendes Erhitzen des nach der Hydrolyse erhaltenen Reaktionsprodukts mit wenig Jod auf 180-250grad und mit Schwefel auf 220-240grad

With diethyl ether; phosphorus pentachloride; xylene;
DOI:10.1021/ja01269a069

Reference yield:

: 124925-46-8
6a,12b-dihydro-6H,7H-benzo[c]phenanthrene-5,8-dione

: 75-16-1
methylmagnesium bromide

: 54986-63-9
5,8-dimethylbenzo[c]phenanthrene

Guidance literature:: With diethyl ether; xylene; aufeinanderfolgendes Erhitzen des nach der Hydrolyse erhaltenen Reaktionsprodukts mit wenig Jod auf 180-250grad und mit Schwefel auf 220-240grad;
DOI:10.1021/ja01269a069