1-ethyl-4-tosylpiperazine

Base Information

• Chemical Name: 1-ethyl-4-tosylpiperazine
• CAS No.: 100800-51-9
• Molecular Formula: C13H20N2O2S
• Molecular Weight: 268.3751
• Mol file: 100800-51-9.mol

Synonyms:1-ethyl-4-tosylpiperazine

Chemical Property of 1-ethyl-4-tosylpiperazine

Chemical Property:

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1-ethyl-4-tosylpiperazine

There total 3 articles about 1-ethyl-4-tosylpiperazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

4-ethylpiperazine (5308-25-8) + toluene-4-sulfonic acid hydrazide (1576-35-8) → 1-ethyl-4-tosylpiperazine (100800-51-9)

Guidance literature:

With tert.-butylhydroperoxide; ammonium iodide; In water; acetonitrile; at 20 ℃; for 16h;

DOI:10.1002/cjoc.201500796

Reference yield: 50.0%

4-ethylpiperazine (5308-25-8) + C33H38O3S → C32H44N2 (1410790-20-3) + 1-ethyl-4-tosylpiperazine (100800-51-9)

Guidance literature:

In ethanol; for 0.5h; Reflux;

DOI:10.1021/jm3013008

Reference yield:

N,N-bis(2-chloroethyl)-p-toluenesulfonamide (42137-88-2) + diethylamine (109-89-7) → 1-ethyl-4-tosylpiperazine (100800-51-9)

Guidance literature:

With ethanol; at 125 ℃; Erh_. des Rktprod_. unter vermindertem Druck auf 250grad;

upstream raw materials:

N,N-bis(2-chloroethyl)-p-toluenesulfonamide

diethylamine

4-ethylpiperazine

toluene-4-sulfonic acid hydrazide

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