2-PHTHALIMIDOLACTOSAMINE, HEPTAACETATE (MIXTURE OF ISOMERS)

Base Information

Chemical Name:2-PHTHALIMIDOLACTOSAMINE, HEPTAACETATE (MIXTURE OF ISOMERS)
CAS No.:129647-37-6
Molecular Formula:C20H25NO5
Molecular Weight:359.4162
Hs Code.:
Mol file:129647-37-6.mol

Synonyms:2-PHTHALIMIDOLACTOSAMINE, HEPTAACETATE (MIXTURE OF ISOMERS);1,3,6-Tri-O-acetyl-4-(2,3,4,6-tetra-O-acetyl-b-D-galactopyranosyl)-2-deoxy-2-phthalimido-a-D-galactopyranose;1,3,6-Tri-O-acetyl-4-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-2-deoxy-2-phthalimido-α-D-galactopyranose;1,3,6-Tri-O-acetyl-4-(2,3,4,6-tetra-O-acetyl-b-D-galactopyranosyl)-2-deoxy-2-phthaliMido-α-D-galactopyranose

Suppliers and Price of 2-PHTHALIMIDOLACTOSAMINE, HEPTAACETATE (MIXTURE OF ISOMERS)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
2-Phthalimidolactosamine,Heptaacetate(MixtureofIsomers)
100mg
$ 205.00

Medical Isotopes, Inc.
2-Phthalimidolactosamine,Heptaacetate(MixtureofIsomers)
100 mg
$ 845.00

Total 6 raw suppliers

Chemical Property of 2-PHTHALIMIDOLACTOSAMINE, HEPTAACETATE (MIXTURE OF ISOMERS)

Chemical Property:

Melting Point:265 - 266 °C
Boiling Point:767.1±60.0 °C(Predicted)
PKA:-2.55±0.20(Predicted)
PSA：249.17000
Density:1.44±0.1 g/cm3(Predicted)
LogP:-0.15980
Solubility.:Chloroform, Dichloromethane, Ethyl Acetate

Purity/Quality:

98%min ^*data from raw suppliers

2-Phthalimidolactosamine,Heptaacetate(MixtureofIsomers) ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Uses 2-Phthalimidolactosamine, Heptaacetate (Mixture of Isomers) (cas# 129647-37-6) is a compound useful in organic synthesis.

Technology Process of 2-PHTHALIMIDOLACTOSAMINE, HEPTAACETATE (MIXTURE OF ISOMERS)

There total 10 articles about 2-PHTHALIMIDOLACTOSAMINE, HEPTAACETATE (MIXTURE OF ISOMERS) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: Acetic acid (2R,3S,4R)-2-acetoxymethyl-5-azido-6-nitrooxy-3-((2S,3R,4S,5S,6R)-3,4,5-triacetoxy-6-acetoxymethyl-tetrahydro-pyran-2-yloxy)-tetrahydro-pyran-4-yl ester

: 68124-18-5,76542-62-6,129647-37-6
1,3,6-tri-O-acetyl-4-O-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-2-deoxy-2-phthalimido-α-D-mannopyranose

Guidance literature:: Multi-step reaction with 3 steps

1: hydrogen / 10percent palladium-charcoal / ethyl acetate / 3000.2 Torr

2: sodium carbonate / aq. ethanol / 2 h / Ambient temperature; pH 9

3: pyridine / 1.) room temperature, overnight, 2.) boiling water-bath, 1 h

With pyridine; hydrogen; sodium carbonate; palladium on activated charcoal; In ethanol; ethyl acetate;
DOI:10.1039/P19810002070

Reference yield:

: 108-24-7
acetic anhydride

: 2-[(3R,4R,5S,6R)-2,4-Dihydroxy-6-hydroxymethyl-5-((2S,3R,4S,5R,6R)-3,4,5-trihydroxy-6-hydroxymethyl-tetrahydro-pyran-2-yloxy)-tetrahydro-pyran-3-yl]-isoindole-1,3-dione

: 129647-37-6
O-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-(1->4)-1,3,6-tri-O-acetyl-2-deoxy-2-phthalimido-α,β-D-glucopyranose

Guidance literature:: With pyridine; at 20 - 100 ℃; for 4.2h;
DOI:10.1016/S0040-4020(98)00294-4

Reference yield:

: 85-44-9
phthalic anhydride

: 68124-18-5,76542-62-6,129647-37-6
1,3,6-tri-O-acetyl-4-O-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-2-deoxy-2-phthalimido-α-D-mannopyranose

Guidance literature:: Multi-step reaction with 2 steps

1: sodium carbonate / aq. ethanol / 2 h / Ambient temperature; pH 9

2: pyridine / 1.) room temperature, overnight, 2.) boiling water-bath, 1 h

With pyridine; sodium carbonate; In ethanol;
DOI:10.1039/P19810002070