5-(Tributylstannyl)-2-(trimethylsilyl)thiazole

Base Information

• Chemical Name: 5-(Tributylstannyl)-2-(trimethylsilyl)thiazole
• CAS No.: 263868-71-9
• Molecular Formula: C18H37NSSiSn
• Molecular Weight: 446.35358
• Hs Code.: 2934100090
• Mol file: 263868-71-9.mol

Synonyms:5-(Tributylstannyl)-2-(trimethylsilyl)thiazole

Chemical Property of 5-(Tributylstannyl)-2-(trimethylsilyl)thiazole

Chemical Property:

• Vapor Pressure: 0mmHg at 25°C
• Boiling Point: 418.052°C at 760 mmHg
• Flash Point: 206.631°C
• PSA: 41.13000
• LogP: 5.74440

Purity/Quality:

99.99%HPLC ^*data from raw suppliers

5-(Tributylstannyl)-2-(trimethylsilyl)thiazole 95% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 5-(Tributylstannyl)-2-(trimethylsilyl)thiazole

There total 2 articles about 5-(Tributylstannyl)-2-(trimethylsilyl)thiazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

tributyltin chloride (1461-22-9) → 5-(tributylstannyl)-2-(trimethylsilyl)thiazole (263868-71-9)

Guidance literature:

2-(trimethylsilyl)thiazole; With n-butyllithium; In diethyl ether; hexane; at -78 ℃; for 0.333333h;

tributyltin chloride; In diethyl ether; hexane; at -78 - 20 ℃; for 1h;

With sodium hydroxide; In diethyl ether; hexane; water;

Reference yield:

tributyltin chloride (1461-22-9) + 2-(trimethylsilyl)thiazole (79265-30-8) → 5-(tributylstannyl)-2-(trimethylsilyl)thiazole (263868-71-9)

Guidance literature:

2-(trimethylsilyl)thiazole; With n-butyllithium; In diethyl ether; at -78 ℃; for 1.5h;

tributyltin chloride; In diethyl ether; at -78 ℃; for 1.25h;

Reference yield:

5-(tributylstannyl)-2-(trimethylsilyl)thiazole (263868-71-9) → 5-(tributylstannanyl)-1,3-thiazole (157025-33-7)

Guidance literature:

With methanol; aluminum oxide; ammonia; In chloroform;

upstream raw materials:

tributyltin chloride

2-(trimethylsilyl)thiazole

Downstream raw materials:

5-(tributylstannanyl)-1,3-thiazole

Refernces

• 1、 -. "HETEROCYCLIC COMPOUNDS". Page/Page column 12. . Retrieved 2008/06/13.