1-(3-AMINOPHENYL)-2,5-DIMETHYLPYRROLE

Base Information

• Chemical Name: 1-(3-AMINOPHENYL)-2,5-DIMETHYLPYRROLE
• CAS No.: 247225-33-8
• Molecular Formula: C12H14N2
• Molecular Weight: 186.257
• Hs Code.: 2933998090
• Mol file: 247225-33-8.mol

Synonyms:TIMTEC-BB SBB010749;1-(3-AMINOPHENYL)-2,5-DIMETHYLPYRROLE;3-(2,5-DIMETHYL-PYRROL-1-YL)-PHENYLAMINE;3-(2,5-dimethyl-1H-pyrrol-1-yl)aniline(SALTDATA: FREE);3-(2,5-DiMethylpyrrol-1-yl)aniline

Chemical Property of 1-(3-AMINOPHENYL)-2,5-DIMETHYLPYRROLE

Chemical Property:

• Vapor Pressure: 3.44E-05mmHg at 25°C
• Boiling Point: 354°C at 760 mmHg
• Flash Point: 167.9°C
• PSA: 30.95000
• Density: 1.06g/cm³
• LogP: 3.25750

Purity/Quality:

98%min ^*data from raw suppliers

3-(2,5-Dimethylpyrrol-1-yl)aniline ^*data from reagent suppliers

Safty Information:

• Pictogram(s): Xi
• Hazard Codes: Xi,Xn
• Statements: 22-41
• Safety Statements: 26-39

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1-(3-AMINOPHENYL)-2,5-DIMETHYLPYRROLE

There total 5 articles about 1-(3-AMINOPHENYL)-2,5-DIMETHYLPYRROLE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

N-(3′-nitrophenyl)-2,5-dimethylpyrrole (32570-23-3) → 3-(2,5-dimethyl-1H-pyrrol-1-yl)aniline (247225-33-8)

Guidance literature:

With iron; acetic acid; In ethanol; water; for 0.3h; Reflux;

DOI:10.1016/j.ejmech.2016.04.022

Reference yield: 83.0%

m-phenylenediamine (108-45-2,64554-26-3,76583-20-5) + 2,5-hexanedione (110-13-4) → 3-(2,5-dimethyl-1H-pyrrol-1-yl)aniline (247225-33-8) + 2,5-dimethyl-1-(3-(2,5-dimethyl-1H-pyrrol-1-yl)phenyl)-1Hpyrrole (201023-86-1)

Guidance literature:

With citric acid; for 0.25h; Milling;

DOI:10.1002/ejoc.201501223

Reference yield: 80.0%

2,5-dimethylfuran (625-86-5) + m-phenylenediamine (108-45-2,64554-26-3,76583-20-5) → 3-(2,5-dimethyl-1H-pyrrol-1-yl)aniline (247225-33-8)

Guidance literature:

With solid acid H form zeolite Y with 2.6 Si/Al catalyst; In toluene; at 150 ℃; for 4h; under 3750.38 Torr; Inert atmosphere;

DOI:10.1021/acscatal.6b02953

upstream raw materials:

m-phenylenediamine

2,5-hexanedione

N-(3′-nitrophenyl)-2,5-dimethylpyrrole

3-nitro-aniline

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