2,4,6-TriMethoxyphenylboronic acid, pinacol ester

Base Information

Chemical Name:2,4,6-TriMethoxyphenylboronic acid, pinacol ester
CAS No.:269410-04-0
Molecular Formula:C15H25BO6
Molecular Weight:294.156
Hs Code.:2931900090
Mol file:269410-04-0.mol

Synonyms:2,4,6-TriMethoxyphenylboronic acid, pinacol ester;4,4,5,5-tetramethyl-2-(2,4,6-trimethoxyphenyl)-1,3,2-dioxaborolane

Suppliers and Price of 2,4,6-TriMethoxyphenylboronic acid, pinacol ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Crysdot
4,4,5,5-Tetramethyl-2-(2,4,6-trimethoxyphenyl)-1,3,2-dioxaborolane 95+%
250mg
$ 424.00

AOBChem
2,4,6-Trimethoxyphenylboronicacidpinacolester 95%
10g
$ 2176.00

Total 14 raw suppliers

Chemical Property of 2,4,6-TriMethoxyphenylboronic acid, pinacol ester

Chemical Property:

PSA：46.15000
LogP:2.01160

Purity/Quality:

99%,98%, ^*data from raw suppliers

4,4,5,5-Tetramethyl-2-(2,4,6-trimethoxyphenyl)-1,3,2-dioxaborolane 95+% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 2,4,6-TriMethoxyphenylboronic acid, pinacol ester

There total 4 articles about 2,4,6-TriMethoxyphenylboronic acid, pinacol ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 67827-56-9
2,4,6-trimethoxychlorobenzene

: 73183-34-3
bis(pinacol)diborane

: 269410-04-0
4,4,5,5-tetramethyl-2-(2,4,6-trimethoxyphenyl)-1,3,2-dioxaborolane

Guidance literature:: With trans dichlorobispyridine palladium (II); potassium acetate; In toluene; at 100 ℃; for 16h; Inert atmosphere;
DOI:10.1002/anie.201103224

Reference yield: 80.0%

: 1131-40-4
2-bromo-1,3,5-trimethoxybenzene

: 73183-34-3
bis(pinacol)diborane

: 269410-04-0
4,4,5,5-tetramethyl-2-(2,4,6-trimethoxyphenyl)-1,3,2-dioxaborolane

Guidance literature:: With potassium acetate; palladium diacetate; In toluene; at 100 ℃; for 16h; Inert atmosphere;
DOI:10.1002/anie.201103224

Reference yield: 20.0%

: 621-23-8
1,2,3-trimethoxybenzene

: 73183-34-3
bis(pinacol)diborane

: 269410-04-0
4,4,5,5-tetramethyl-2-(2,4,6-trimethoxyphenyl)-1,3,2-dioxaborolane

Guidance literature:: With (1,5-cyclooctadiene)(methoxy)iridium(I) dimer; cyclopentyl methyl ether; 1,1'-di(pyridin-2-yl)-1,1',3,3'-tetrahydro-2,2'-bibenzo[d][1,3,2]diazaborole; at 150 ℃; for 24h; Schlenk technique; Inert atmosphere;
DOI:10.1021/jacs.5b05252