1,2,3,4-tetrahydro-2-methyl-1-oxo-, methyl ester 2-Naphthalenecarboxylic acid

Base Information

• Chemical Name: 1,2,3,4-tetrahydro-2-methyl-1-oxo-, methyl ester 2-Naphthalenecarboxylic acid
• CAS No.: 54125-61-0
• Molecular Formula: C13H14O3
• Molecular Weight: 218.252
• Mol file: 54125-61-0.mol

Synonyms:1,2,3,4-tetrahydro-2-methyl-1-oxo-, methyl ester 2-Naphthalenecarboxylic acid;methyl 2-methyl-1-oxo-1,2,3,4-tetrahydronaphthalene-2-carboxylate

Chemical Property of 1,2,3,4-tetrahydro-2-methyl-1-oxo-, methyl ester 2-Naphthalenecarboxylic acid

Chemical Property:

• PSA: 43.37000
• LogP: 1.99480
• Storage Temp.: Sealed in dry,Room Temperature
• Solubility.: Chloroform (Slightly, Sonicated), DMSO (Slightly), Methanol (Slightly)

Purity/Quality:

97% ^*data from raw suppliers

Methyl1,2,3,4-tetrahydro-2-methyl-1-oxo-2-naphthalenecarboxylate 98% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Uses: 2-Methoxycarbonyl-2-methyltetralone can be prepared as prostaglandin I2 agonists.

Technology Process of 1,2,3,4-tetrahydro-2-methyl-1-oxo-, methyl ester 2-Naphthalenecarboxylic acid

There total 1 articles about 1,2,3,4-tetrahydro-2-methyl-1-oxo-, methyl ester 2-Naphthalenecarboxylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

allyl 2-methyl-1-oxo-1,2,3,4-tetrahydronaphthalene-2-carboxylate (460315-98-4) + methyl iodide (74-88-4) → 2-methyl-1-tetralone (1590-08-5) + 2-methyl-1-oxo-1,2,3,4-tetrahydronaphthalene-2-carboxylic acid methyl ester (54125-61-0) + 1-allyl-1-hydroxy-2-methyl-1,2,3,4-tetrahydro-naphthalene-2-carboxylic acid methyl ester

Guidance literature:

allyl 2-methyl-1-oxo-1,2,3,4-tetrahydronaphthalene-2-carboxylate; With (2,2'-bipyridine)nickel(II) dibromide; tetrabutylammonium tetrafluoroborate; In N,N-dimethyl-formamide; Electrolysis;

methyl iodide; With potassium carbonate; In N,N-dimethyl-formamide; Further stages.;

DOI:10.1002/1099-0690(200207)2002:14<2257::AID-EJOC2257>3.0.CO;2-S

Reference yield: 91.6%

2-methyl-1-oxo-1,2,3,4-tetrahydronaphthalene-2-carboxylic acid methyl ester (54125-61-0) → 2-methyl-1-tetralone (1590-08-5)

Guidance literature:

With hydrogen bromide; In water; at 110 ℃; for 5h;

Reference yield: 25.0%

2-methyl-1-oxo-1,2,3,4-tetrahydronaphthalene-2-carboxylic acid methyl ester (54125-61-0) → 2-methyl-1-tetralone (1590-08-5) + methyl 4-hydroxy-3-methyl-1-naphthoate + ethyl 4-hydroxy-3-methyl-1-naphthoate

Guidance literature:

With lithium hexamethyldisilazane; at -78 - 20 ℃;

DOI:10.1002/ejoc.201300102

upstream raw materials:

allyl 2-methyl-1-oxo-1,2,3,4-tetrahydronaphthalene-2-carboxylate

methyl iodide

Downstream raw materials:

2-methyl-1-tetralone

Toluene-4-sulfonic acid 2-methyl-1-oxo-1,2,3,4-tetrahydro-naphthalen-2-ylmethyl ester

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