N-[(1S,2S)-2-aMino-1,2-bis(4-Methoxyphenyl)ethyl]-4-Methyl-BenzenesulfonaMide

Base Information

• Chemical Name: N-[(1S,2S)-2-aMino-1,2-bis(4-Methoxyphenyl)ethyl]-4-Methyl-BenzenesulfonaMide
• CAS No.: 887924-07-4
• Molecular Formula: C23H26N2O4S
• Molecular Weight: 426.536
• Mol file: 887924-07-4.mol

Synonyms:N-[(1S,2S)-2-aMino-1,2-bis(4-Methoxyphenyl)ethyl]-4-Methyl-BenzenesulfonaMide

Chemical Property of N-[(1S,2S)-2-aMino-1,2-bis(4-Methoxyphenyl)ethyl]-4-Methyl-BenzenesulfonaMide

Chemical Property:

• Boiling Point: 603.6±65.0 °C(Predicted)
• PKA: 10.57±0.50(Predicted)
• PSA: 99.03000
• Density: 1.227±0.06 g/cm3(Predicted)
• LogP: 5.90380

Purity/Quality:

99% ^*data from raw suppliers

N-[(1S,2S)-2-Amino-1,2-bis(4-methoxyphenyl)ethyl]-4-methylbenzenesulfonamide 95%+ ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
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Technology Process of N-[(1S,2S)-2-aMino-1,2-bis(4-Methoxyphenyl)ethyl]-4-Methyl-BenzenesulfonaMide

There total 1 articles about N-[(1S,2S)-2-aMino-1,2-bis(4-Methoxyphenyl)ethyl]-4-Methyl-BenzenesulfonaMide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

p-toluenesulfonyl chloride (98-59-9) + (1S,2S)-1,2-bis(4-methoxyphenyl)ethane-1,2-diamine (58520-04-0,117106-36-2) → (1S,2S)-N-p-toluenesulfonyl-1,2-di(4-methoxyphenyl)ethylenediamine (887924-07-4)

Guidance literature:

With triethylamine; In dichloromethane; at 0 - 20 ℃; for 1.5 - 26h;

Reference yield:

(1S,2S)-N-p-toluenesulfonyl-1,2-di(4-methoxyphenyl)ethylenediamine (887924-07-4) + [ruthenium(II)(η6-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]2 (52462-29-0) → C10H14*C23H26N2O4S*Cl(1-)*Ru(1+)

Guidance literature:

With triethylamine; In isopropyl alcohol; at 70 - 90 ℃; for 1 - 4h;

Reference yield:

(1S,2S)-N-p-toluenesulfonyl-1,2-di(4-methoxyphenyl)ethylenediamine (887924-07-4) + [{(η6-p-cymene)RuIICl2}2] → C33H40ClN2O4RuS

Guidance literature:

In N,N-dimethyl-formamide; at 20 ℃; for 0.0833333 - 0.25h;

upstream raw materials:

p-toluenesulfonyl chloride

(1S,2S)-1,2-bis(4-methoxyphenyl)ethane-1,2-diamine

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