3-Bromo-2-formyltoluene, 6-Bromo-o-tolualdehyde

Base Information

• Chemical Name: 3-Bromo-2-formyltoluene, 6-Bromo-o-tolualdehyde
• CAS No.: 176504-70-4
• Molecular Formula: C8H7BrO
• Molecular Weight: 199.047
• Hs Code.: 2913000090
• Mol file: 176504-70-4.mol

Synonyms:2-Bromo-6-methylbenzaldehyde 96%;3-Bromo-2-formyltoluene, 6-Bromo-o-tolualdehyde;2-broMo-6-Methylbenzaldehyde;2-Bromo-6-methylbenzaldehyde96%

Chemical Property of 3-Bromo-2-formyltoluene, 6-Bromo-o-tolualdehyde

Chemical Property:

• PSA: 17.07000
• LogP: 2.57000

Purity/Quality:

99%, ^*data from raw suppliers

2-Bromo-6-methylbenzaldehyde ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 3-Bromo-2-formyltoluene, 6-Bromo-o-tolualdehyde

There total 13 articles about 3-Bromo-2-formyltoluene, 6-Bromo-o-tolualdehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

methyl iodide (74-88-4) → 2-bromo-6-methylbenzaldehyde (176504-70-4)

Guidance literature:

2-(2,6-dibromophenyl)-1,3-dioxane; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 1.91667h;

methyl iodide; In tetrahydrofuran; hexane; at -78 - 20 ℃; for 1.91667h;

With hydrogenchloride; water; In tetrahydrofuran; hexane; at 20 ℃; for 1.5h;

Reference yield: 96.0%

2-(2,6-dibromophenyl)-1,3-dioxane + methyl iodide (74-88-4) → 2-bromo-6-methylbenzaldehyde (176504-70-4)

Guidance literature:

2-(2,6-dibromophenyl)-1,3-dioxane; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 1.5h;

methyl iodide; In tetrahydrofuran; hexane; at -78 - 20 ℃; for 1.91667h; Further stages.;

DOI:10.1002/chem.200601142

Reference yield: 90.0%

2-bromo-6-methylbenzaldehyde O-methyloxime → 2-bromo-6-methylbenzaldehyde (176504-70-4)

Guidance literature:

With formaldehyd; toluene-4-sulfonic acid; In tetrahydrofuran; water; at 100 ℃; for 0.25h; Microwave irradiation;

DOI:10.1021/jo200853j

upstream raw materials:

meta-bromotoluene

hexamethylenetetramine

methyl iodide

2-methylphenyl aldehyde

Downstream raw materials:

C₁₅H₂₀BrNOSe

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