Carbamic acid, N-[(6-hydroxybenzo[b]thien-2-yl)iminomethyl]-, 1,1-dimethylethyl ester

Base Information

• Chemical Name: Carbamic acid, N-[(6-hydroxybenzo[b]thien-2-yl)iminomethyl]-, 1,1-dimethylethyl ester
• CAS No.: 947590-65-0
• Molecular Formula: C14H16N2O3S
• Molecular Weight: 292.359
• Mol file: 947590-65-0.mol

Synonyms:Carbamic acid, N-[(6-hydroxybenzo[b]thien-2-yl)iminomethyl]-, 1,1-dimethylethyl ester

Chemical Property of Carbamic acid, N-[(6-hydroxybenzo[b]thien-2-yl)iminomethyl]-, 1,1-dimethylethyl ester

Chemical Property:

• PSA: 110.65000
• Density: 1.27g/cm³
• LogP: 3.94760

Purity/Quality:

95% ^*data from raw suppliers

1,1-DIMETHYLETHYL-N-[(6-HYDROXYBENZO[B]THIEN-2-YL)IMINOMETHYL]CARBAMIC ACID ESTER 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
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MSDS Files:

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Technology Process of Carbamic acid, N-[(6-hydroxybenzo[b]thien-2-yl)iminomethyl]-, 1,1-dimethylethyl ester

There total 1 articles about Carbamic acid, N-[(6-hydroxybenzo[b]thien-2-yl)iminomethyl]-, 1,1-dimethylethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

N'-t-Boc-6-allyloxybenzothiophene-2-carboxamidine (947590-64-9) → N'-t-Boc-6-hydroxybenzothiophene-2-carboxamidine (947590-65-0)

Guidance literature:

N'-t-Boc-6-allyloxybenzothiophene-2-carboxamidine; With tetrakis(triphenylphosphine) palladium⁽⁰⁾; phenylsilane; In dichloromethane; at 0 - 20 ℃; Inert atmosphere;

With water; In dichloromethane;

DOI:10.1021/jm901475e

Reference yield: 86.0%

N'-t-Boc-6-hydroxybenzothiophene-2-carboxamidine (947590-65-0) + 1-(Bromomethyl)-3-fluorobenzene (456-41-7) → C21H21FN2O3S (1209467-18-4)

Guidance literature:

With potassium carbonate; In N,N-dimethyl-formamide; Reflux;

DOI:10.1021/jm901475e

Reference yield: 81.0%

N'-t-Boc-6-hydroxybenzothiophene-2-carboxamidine (947590-65-0) + methyl 4-chloromandelate (32174-34-8,63096-36-6,104420-79-3,13305-19-6) → C23H23ClN2O5S (947590-61-6)

Guidance literature:

With triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; at 20 ℃; for 15.25h;

upstream raw materials:

N'-t-Boc-6-allyloxybenzothiophene-2-carboxamidine

Downstream raw materials:

C₂₃H₂₃ClN₂O₅S

C₂₅H₂₇ClN₂O₅S

C₂₁H₂₁FN₂O₃S

C₂₁H₂₁FN₂O₃S

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