β-naphthyl o-biphenyl ketone

Base Information

Chemical Name:β-naphthyl o-biphenyl ketone
CAS No.:97191-81-6
Molecular Formula:C₂₃H₁₆O
Molecular Weight:308.379
Hs Code.:

Synonyms:β-naphthyl o-biphenyl ketone

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Chemical Property of β-naphthyl o-biphenyl ketone

Chemical Property:

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Technology Process of β-naphthyl o-biphenyl ketone

There total 6 articles about β-naphthyl o-biphenyl ketone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 4688-76-0
2-Biphenylboronic acid

: 2243-83-6
2-naphthaloyl chloride

: 97191-81-6
β-naphthyl o-biphenyl ketone

Guidance literature:: With bis-triphenylphosphine-palladium(II) chloride; potassium phosphate tribasic trihydrate; In toluene; at 110 ℃; for 4h; Inert atmosphere; Schlenk technique;
DOI:10.1021/acs.orglett.5b00797

Reference yield:

: 947-84-2
2-Biphenylcarboxylic acid

: 97191-81-6
β-naphthyl o-biphenyl ketone

Guidance literature:: Multi-step reaction with 4 steps

1.1: lithium aluminium tetrahydride / tetrahydrofuran / 4 h / 0 - 20 °C / Inert atmosphere

2.1: manganese(IV) oxide / dichloromethane / Reflux

3.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / -50 °C / Inert atmosphere

3.2: 3 h / -50 - 20 °C / Inert atmosphere

4.1: manganese(IV) oxide / dichloromethane / Reflux

With manganese(IV) oxide; lithium aluminium tetrahydride; n-butyllithium; In tetrahydrofuran; hexane; dichloromethane;
DOI:10.1002/ejoc.201901278

Reference yield:

: 2928-43-0
2-biphenylmethanol

: 97191-81-6
β-naphthyl o-biphenyl ketone

Guidance literature:: Multi-step reaction with 3 steps

1.1: manganese(IV) oxide / dichloromethane / Reflux

2.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / -50 °C / Inert atmosphere

2.2: 3 h / -50 - 20 °C / Inert atmosphere

3.1: manganese(IV) oxide / dichloromethane / Reflux

With manganese(IV) oxide; n-butyllithium; In tetrahydrofuran; hexane; dichloromethane;
DOI:10.1002/ejoc.201901278