C₉H₁₀ClNO*C₈H₈O₃

Base Information

• Chemical Name: C₉H₁₀ClNO*C₈H₈O₃
• CAS No.: 1425925-82-1
• Molecular Formula: C₈H₈O₃*C₉H₁₀ClNO
• Molecular Weight: 335.787
• Mol file: 1425925-82-1.mol

Synonyms:C₉H₁₀ClNO*C₈H₈O₃

Chemical Property of C₉H₁₀ClNO*C₈H₈O₃

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of C₉H₁₀ClNO*C₈H₈O₃

There total 3 articles about C₉H₁₀ClNO*C₈H₈O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

rel-(1R,2S)-1-amino-5-chloroindan-2-ol + (R)-Mandelic Acid (611-71-2) → C9H10ClNO*C8H8O3 (1425925-82-1)

Guidance literature:

In methanol; at 20 ℃; Reflux;

Reference yield:

rel-(1aR,6aS)-4-chloro-6,6a-dihydro-1aH-indeno[1,2-b]oxirene → C9H10ClNO*C8H8O3 (1425925-82-1)

Guidance literature:

Multi-step reaction with 2 steps

1.1: acetonitrile / hexane / 1 h / -40 - 20 °C

1.2: 20 - 100 °C / Inert atmosphere

2.1: methanol / 20 °C / Reflux

With acetonitrile; In methanol; hexane;

Reference yield:

6-chloro-1H-indene (3970-52-3) → C9H10ClNO*C8H8O3 (1425925-82-1)

Guidance literature:

Multi-step reaction with 3 steps

1.1: 4-(3-phenylpropyl)pyridine-N-oxide; (-)-chloro((1R,2R)-4,4',6,6'-tetra-tert-butyl-2,2'-[cyclohexane-1,2-diylbis(nitrilomethylidyne)]diphenolato)manganese(III); sodium hypochlorite / dichloromethane; water / 2 h / 0 - 20 °C

2.1: acetonitrile / hexane / 1 h / -40 - 20 °C

2.2: 20 - 100 °C / Inert atmosphere

3.1: methanol / 20 °C / Reflux

With sodium hypochlorite; (-)-chloro((1R,2R)-4,4',6,6'-tetra-tert-butyl-2,2'-[cyclohexane-1,2-diylbis(nitrilomethylidyne)]diphenolato)manganese(III); acetonitrile; 4-(3-phenylpropyl)pyridine-N-oxide; In methanol; hexane; dichloromethane; water;

upstream raw materials:

(R)-Mandelic Acid

6-chloro-1H-indene

Downstream raw materials:

(1R,2S)-5-chloro-2-methoxyindan-1-amine